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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4740-52-7
合成路线
（共 12 条）
1338363-02-2
+
98-80-6
苯硼酸
→
反应条件
4740-52-7
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate in tetrahydrofuran; water Suzuki coupling; Heating;
参考文献
Mathew, Sanyo M.; Hartley, C. Scott
Macromolecules, 2011 , vol. 44, # 21 p. 8425 - 8432
1338363-01-1
→
反应条件
4740-52-7
反应条件
1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating 2: pyridine / dichloromethane 3: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating View Scheme
参考文献
Mathew, Sanyo M.; Hartley, C. Scott
Macromolecules, 2011 , vol. 44, # 21 p. 8425 - 8432
14205-96-0
→
反应条件
4740-52-7
反应条件
1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating 2: pyridine / dichloromethane 3: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating 4: pyridine / dichloromethane 5: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating View Scheme
参考文献
Mathew, Sanyo M.; Hartley, C. Scott
Macromolecules, 2011 , vol. 44, # 21 p. 8425 - 8432
90-43-7
联苯-2-酚
→
反应条件
4740-52-7
反应条件
1: boron trichloride 2: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating 3: pyridine / dichloromethane 4: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating 5: pyridine / dichloromethane 6: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating View Scheme
参考文献
Mathew, Sanyo M.; Hartley, C. Scott
Macromolecules, 2011 , vol. 44, # 21 p. 8425 - 8432
4731-96-8
→
反应条件
4740-52-7
反应条件
1: pyridine / dichloromethane 2: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating 3: pyridine / dichloromethane 4: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / Heating View Scheme
参考文献
Mathew, Sanyo M.; Hartley, C. Scott
Macromolecules, 2011 , vol. 44, # 21 p. 8425 - 8432
2113-51-1
2-碘联苯
+
2236-52-4
2,2-二碘代联苯
→
反应条件
4740-52-7
反应条件
copper T=265 - 270°C;
参考文献
Ibuki,E. et al.
Bulletin of the Chemical Society of Japan, 1975 , vol. 48, p. 1868 - 1874
39655-15-7
→
反应条件
217-59-4
9,10-苯并菲
+
84-15-1
邻三联苯
+
4740-52-7
反应条件
copper T=275 - 280°C; 2 h;
参考文献
Ibuki, Eiichi; Ozasa, Shigeru; Fujioka, Yasuhiro; Kitamura, Hirohiko
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 5 p. 1468 - 1476
2436-96-6
2,2'-二硝基联苯
→
反应条件
4740-52-7
反应条件
1: Fe / benzene 2: (i) NaNO2, H2SO4, (ii) aq. KI 3: Cu / 265 - 270 °C View Scheme
参考文献
Ibuki,E. et al.
Bulletin of the Chemical Society of Japan, 1975 , vol. 48, p. 1868 - 1874
16291-37-5
→
反应条件
4740-52-7
反应条件
n-butyllithium in diethyl ether
参考文献
Wittig,G.; Klar,G.
Justus Liebigs Annalen der Chemie, 1967 , vol. 704, p. 91 - 108
16291-32-0
→
反应条件
4740-52-7
反应条件
diethyl ether; iron(II) chloride
参考文献
Wittig; Lehmann
Chemische Berichte, 1957 , vol. 90, p. 875,880
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