6-甲氧基-3H-异苯并呋喃-1-酮合成路线 (共 34 条)
反应条件
potassium carbonate in acetonitrile
T=35°C; 16 h;
参考文献
Blizzard, Timothy A.; Mosley, Ralph T.; Birzin, Elizabeth T.; Chan, Wanda; Hammond, Milton L.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 5 p. 1317 - 1321
反应条件
iodine; mercury(II) oxide in benzene
Ambient temperatureIrradiation;
参考文献
Kobayashi, Kazuhiro; Itoh, Masahito; Suginome, Hiroshi
Tetrahedron Letters, 1987 , vol. 28, # 29 p. 3369 - 3372
反应条件
1: aqueous sulfuric acid / ueber das Diazoniumsalz
2: aq. NaOH solution
View Scheme
参考文献
Vaughan; Baird
Journal of the American Chemical Society, 1946 , vol. 68, p. 1314
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Tirouflet
Bulletin de la Societe Scientifique de Bretagne, 1951 , vol. 26, p. Sonderheft 5, S. 7, 96
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1952 , vol. 235, p. 962
参考文献
Vaughan; Baird
Journal of the American Chemical Society, 1946 , vol. 68, p. 1314
Full Text View citing articles Show Details
Tirouflet
Bulletin de la Societe Scientifique de Bretagne, 1951 , vol. 26, p. Sonderheft 5, S. 7, 96
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1952 , vol. 235, p. 962
反应条件
3,4-dimethoxybenzylidenemethylamine methiodide in dimethyl sulfoxide
T=130°C; 0.166667 h;
参考文献
Chiefari, John; Janowski, Wit K.; Prager, Rolf H.
Heterocycles, 1989 , vol. 28, # 2 p. 863 - 867
参考文献
Leblois, Danielle; Piessard, Sylvie; Baut, Guillaume Le; Kumar, Piyush; Brion, Jean-Daniel; et al.
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 229 - 238
反应条件
chloromethylation reaction;
参考文献
Leblois, Danielle; Piessard, Sylvie; Baut, Guillaume Le; Kumar, Piyush; Brion, Jean-Daniel; et al.
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 229 - 238
反应条件
manganese(IV) oxide in dichloromethane
Ambient temperatureovernight;
参考文献
Bhattacharjee, Debkumar; Popp, Frank D.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 315 - 320
反应条件
in dimethyl sulfoxide
T=130°C; 0.166667 h;
参考文献
Chiefari, John; Janowski, Wit K.; Prager, Rolf H.
Heterocycles, 1989 , vol. 28, # 2 p. 863 - 867
反应条件
[Cp*Ir(6,6’-(OH)2bpy)(H2O)][OTf]2 in water
6 h; Inert atmosphereRefluxGreen chemistry; Overall yield = 63 percentSpectr.;
参考文献
Fujita, Ken-Ichi; Ito, Wataru; Yamaguchi, Ryohei
ChemCatChem, 2014 , vol. 6, # 1 p. 109 - 112