反应条件
1: 78 percent / bis(2-oxo-3-oxazolidinyl)phosphinic chloride; diisopropylethylamine / toluene / 16.5 h / 85 °C 2: 90 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 4.5 h / 0 - 20 °C 3: 95 percent / aq. HF / acetonitrile / 6 h / 20 °C 4: 5 percent / aq. HNO3; acetic acid / 0.02 h / 20 °C View Scheme
参考文献
Andrus, Merritt B.; Meredith, Erik L.; Simmons, Bryon L.; Sekhar, B. B. V. Soma; Hicken, Erik J.
Organic Letters, 2002 , vol. 4, # 20 p. 3549 - 3552
