1-乙炔-4-((4-(苯基乙炔)苯基)乙炔)苯合成路线 （共 2 条）
反应条件
1: [Pd2(dba)3*CHCl3]; PPh3; Et3N / CuI / 1 h / 20 °C
2: [Pd2(dba)3*CHCl3]; PPh3; Et3N / CuI / 20 °C
3: NaOH; water / ethanol; tetrahydrofuran / 1 h / 20 °C
4: [Pd2(dba)3*CHCl3]; PPh3; Et3N / CuI / 20 °C
5: Bu4NF / tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Ljungdahl, Thomas; Pettersson, Karin; Albinsson, Bo; Martensson, Jerker
European Journal of Organic Chemistry, 2006 , # 14 p. 3087 - 3096
反应条件
1: [Pd2(dba)3*CHCl3]; PPh3; Et3N / CuI / 20 °C
2: NaOH; water / ethanol; tetrahydrofuran / 1 h / 20 °C
3: [Pd2(dba)3*CHCl3]; PPh3; Et3N / CuI / 20 °C
4: Bu4NF / tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Ljungdahl, Thomas; Pettersson, Karin; Albinsson, Bo; Martensson, Jerker
European Journal of Organic Chemistry, 2006 , # 14 p. 3087 - 3096
