2-羟基-N-苯基乙酰胺合成路线 (共 30 条)
参考文献
Ramirez,F. et al.
Journal of the American Chemical Society, 1970 , vol. 92, p. 6935 - 6942
反应条件
N(Et)4ClO4; methyl iodide in N,N-dimethyl-formamide
T=15°C; mercury catode; Further byproducts given;
参考文献
Casadei, Maria Antonietta; Cesa, Stefania; Inesi, Achille; Moracci, Franco Micheletti
Journal of Chemical Research, Miniprint, 1995 , # 5 p. 1064 - 1079
参考文献
Grimmel; Guenther; Morgan
Journal of the American Chemical Society, 1946 , vol. 68, p. 539
反应条件
in toluene
18 h; Heating;
参考文献
Khalaj, A.; Nahid, E.
Synthesis, 1985 , # 12 p. 1153 - 1155
反应条件
tetraethyl ethylenecarboxylate; N(Et)4ClO4 in N,N-dimethyl-formamide
electrolysis, Hg cathode, Pt anode;
参考文献
Casadei, Maria Antonietta; Cesa, Stefania; Inesi, Achille
Tetrahedron, 1995 , vol. 51, # 20 p. 5891 - 5900
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
T=15°C; mercury catode; Further byproducts given;
参考文献
Casadei, Maria Antonietta; Cesa, Stefania; Inesi, Achille; Moracci, Franco Micheletti
Journal of Chemical Research, Miniprint, 1995 , # 5 p. 1064 - 1079
反应条件
1: CH2Cl2 / 2 h / 0 °C
2: 4 percent / TEAP / dimethylformamide / 15 °C / mercury catode
View Scheme
参考文献
Casadei, Maria Antonietta; Cesa, Stefania; Inesi, Achille; Moracci, Franco Micheletti
Journal of Chemical Research, Miniprint, 1995 , # 5 p. 1064 - 1079
反应条件
1: copper diacetate / 1,1-dimethylpropan-1-ol / 8 h / 140 °C / Inert atmosphere
2: copper diacetate / 1,1-dimethylpropan-1-ol / 10 h / 140 °C / Inert atmosphere
View Scheme
参考文献
Zhang, Min; Imm, Sebastian; Baehn, Sebastian; Neubert, Lorenz; Neumann, Helfried; Beller, Matthias
Angewandte Chemie - International Edition, 2012 , vol. 51, # 16 p. 3905 - 3909
参考文献
Shapiro et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 6322,6323
反应条件
sodium hydroxide in 1,4-dioxane; water
27 h; Heating;
参考文献
Ono; Hayakawa; Tamura
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 5 p. 1176 - 1181