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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
474657-72-2
合成路线
（共 11 条）
80693-54-5
→
反应条件
474657-72-2
反应条件
water; sodium hydroxide in ethanol T=20°C; 48 h;
参考文献
Adla, Santosh Kumar; Golz, Gregor; Jones, Peter G.; Lindel, Thomas
Synthesis, 2010 , # 13 art. no. C02610SS, p. 2161 - 2170
1353012-45-9
→
反应条件
474657-72-2
反应条件
tri-n-butyl-tin hydride in toluene T=65°C; 2 h;
参考文献
Isaji, Hisaaki; Nakazaki, Atsuo; Isobe, Minoru; Nishikawa, Toshio
Chemistry Letters, 2011 , vol. 40, # 10 p. 1079 - 1081
951322-09-1
→
反应条件
474657-72-2
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 0.5 h;
参考文献
Kim, Jin-Sung; Padnya, Anshul; Weltzin, Maegan; Edmonds, Brian W.; Schulte, Marvin K.; Glennon, Richard A.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 17 p. 4855 - 4860
863885-34-1
→
反应条件
474657-72-2
反应条件
1: 61 percent / N-bromosuccinimide; acetic acid; formic acid / 0.5 h / 20 °C 2: NaOH / ethanol / 24 h / Heating View Scheme
参考文献
Lindel, Thomas; Braeuchle, Laura; Golz, Gregor; Boehrer, Petra
Organic Letters, 2007 , vol. 9, # 2 p. 283 - 286
61-49-4
N(omega)-甲基色胺
→
反应条件
474657-72-2
反应条件
1.1: acetic anhydride / 1 h / 60 °C 1.2: 90 percent / CH2Cl2 / 1.5 h / 20 °C 2.1: t-BuOCl; triethylamine / tetrahydrofuran / 0.5 h / -78 °C 2.2: tetrahydrofuran / 1.5 h / -78 - 20 °C 2.3: H2O2; NaOH / tetrahydrofuran; H2O / 1 h / 20 °C 3.1: 61 percent / N-bromosuccinimide; acetic acid; formic acid / 0.5 h / 20 °C 4.1: NaOH / ethanol / 24 h / Heating View Scheme
参考文献
Lindel, Thomas; Braeuchle, Laura; Golz, Gregor; Boehrer, Petra
Organic Letters, 2007 , vol. 9, # 2 p. 283 - 286
598-25-4
3-甲基-1,2-丁二烯
→
反应条件
474657-72-2
反应条件
1.1: 18 h / 20 °C 2.1: t-BuOCl; triethylamine / tetrahydrofuran / 0.5 h / -78 °C 2.2: tetrahydrofuran / 1.5 h / -78 - 20 °C 2.3: H2O2; NaOH / tetrahydrofuran; H2O / 1 h / 20 °C 3.1: 61 percent / N-bromosuccinimide; acetic acid; formic acid / 0.5 h / 20 °C 4.1: NaOH / ethanol / 24 h / Heating View Scheme
参考文献
Lindel, Thomas; Braeuchle, Laura; Golz, Gregor; Boehrer, Petra
Organic Letters, 2007 , vol. 9, # 2 p. 283 - 286
54268-27-8
→
反应条件
474657-72-2
反应条件
1.1: t-BuOCl; triethylamine / tetrahydrofuran / 0.5 h / -78 °C 1.2: tetrahydrofuran / 1.5 h / -78 - 20 °C 1.3: H2O2; NaOH / tetrahydrofuran; H2O / 1 h / 20 °C 2.1: 61 percent / N-bromosuccinimide; acetic acid; formic acid / 0.5 h / 20 °C 3.1: NaOH / ethanol / 24 h / Heating View Scheme
参考文献
Lindel, Thomas; Braeuchle, Laura; Golz, Gregor; Boehrer, Petra
Organic Letters, 2007 , vol. 9, # 2 p. 283 - 286
55454-18-7
→
反应条件
474657-72-2
反应条件
1.1: t-BuOCl; triethylamine / tetrahydrofuran / 0.5 h / -78 °C 1.2: tetrahydrofuran / 1.5 h / -78 - 20 °C 1.3: H2O2; NaOH / tetrahydrofuran; H2O / 1 h / 20 °C 2.1: 61 percent / N-bromosuccinimide; acetic acid; formic acid / 0.5 h / 20 °C 3.1: NaOH / ethanol / 24 h / Heating View Scheme
参考文献
Lindel, Thomas; Braeuchle, Laura; Golz, Gregor; Boehrer, Petra
Organic Letters, 2007 , vol. 9, # 2 p. 283 - 286
52415-29-9
6-溴吲哚
→
反应条件
474657-72-2
反应条件
1: diethyl ether 2: triethylamine / N,N-dimethyl-formamide 3: tert-butylhypochlorite / tetrahydrofuran 4: trifluoroacetic acid / dichloromethane View Scheme
参考文献
German, Nadezhda; Kim, Jin-Sung; Jain, Atul; Dukat, Malgorzata; Pandya, Anshul; Ma, Yilong; Weltzin, Maegan; Schulte, Marvin K.; Glennon, Richard A.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 20 p. 7259 - 7267
209168-89-8
→
反应条件
474657-72-2
反应条件
1: tert-butylhypochlorite / tetrahydrofuran 2: trifluoroacetic acid / dichloromethane View Scheme
参考文献
German, Nadezhda; Kim, Jin-Sung; Jain, Atul; Dukat, Malgorzata; Pandya, Anshul; Ma, Yilong; Weltzin, Maegan; Schulte, Marvin K.; Glennon, Richard A.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 20 p. 7259 - 7267
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