N-BOC-3A,4,7,7A-四氢异吲哚合成路线 (共 3 条)
反应条件
1: 4-cyclohexene-1,2-dicarboximide With lithium aluminium tetrahydride in tetrahydrofuran
24 h; Heating;
2: di-tert-butyl dicarbonate in dichloromethane
1 h; Further stages.;
参考文献
Johnson, Timothy A.; Jang, Doo Ok; Slafer, Brian W.; Curtis, Michael D.; Beak, Peter
Journal of the American Chemical Society, 2002 , vol. 124, # 39 p. 11689 - 11698
反应条件
triethylamine in tetrahydrofuran
T=20°C; 7 h;
参考文献
Shulman; Makarov; Ogawa; Romesberg; Keinan
Journal of the American Chemical Society, 2000 , vol. 122, # 44 p. 10743 - 10753
反应条件
1: LiAlH4 / tetrahydrofuran; diethyl ether / Heating
2: Et3N / tetrahydrofuran / 7 h / 20 °C
View Scheme
参考文献
Shulman; Makarov; Ogawa; Romesberg; Keinan
Journal of the American Chemical Society, 2000 , vol. 122, # 44 p. 10743 - 10753