N-(4-氯苯基)苯磺酰胺合成路线 （共 25 条）
反应条件
1: 1) NaH / 1) DMF, room temperature, 30 min.; 2) room temperature, overnight 2: NaOH / ethanol; H2O / 2 h / Heating View Scheme
参考文献
DeRuiter, Jack; Borne, Ronald F.; Mayfield, Charles A.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 1 p. 145 - 151
反应条件
C6H5Hg(1+)*CF3COO(1-) = C6H5HgOCOCF3 in dimethyl sulfoxide T=25°C; Equilibrium constant;
参考文献
Kravtsov, D. N.; Peregudov, A. S.; Ivanov, V. F.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 3 p. 468 - 474
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 3 p. 522 - 528
反应条件
C6H5Hg(1+)*CF3COO(1-) = C6H5HgOCOCF3 in dimethyl sulfoxide T=25°C; Equilibrium constant;
参考文献
Kravtsov, D. N.; Peregudov, A. S.; Ivanov, V. F.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 3 p. 468 - 474
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 3 p. 522 - 528
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in acetonitrile
T=70°C; 8 h; Inert atmosphere;
参考文献
Wang, Xiang; Guram, Anil; Ronk, Michael; Milne, Jacqueline E.; Tedrow, Jason S.; Faul, Margaret M.
Tetrahedron Letters, 2012 , vol. 53, # 1 p. 7 - 10
反应条件
ammonium hydroxide; iron in methanol
T=25°C; Reduction; condensation; 1 h; sonication;
参考文献
Chandrasekhar; Narsihmulu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7969 - 7972
反应条件
tetrabutyl ammonium fluoride; copper diacetate; potassium carbonate in isopropyl alcohol
T=90°C; 12 h;
参考文献
Pan, Changduo; Cheng, Jiang; Wu, Huayue; Ding, Jinchang; Liu, Miaochang
Synthetic Communications, 2009 , vol. 39, # 12 p. 2082 - 2092
参考文献
Ludwig, Miroslav; Pytela, Oldrich; Javurkova, Helena; Vecera, Miroslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 12 p. 2900 - 2908
反应条件
sulfur dioxide
T=-70°C; bei Elektrolyse (an der Anode);
参考文献
Gebauer-Fuelnegg; Jusa
Monatshefte fuer Chemie, 1928 , vol. 50, p. 65
反应条件
1: sulfuryl chloride / 0.05 h / 0 °C / 15 Torr
2: Et3N / CH2Cl2 / 3 h / 0 °C
3: 1.) LDA, 2.) O2 / 1.) THF, RT, 4 h, 2.) THF, RT, 20 h
View Scheme
参考文献
Barbieri, Anna; Montevecchi, Pier Carlo; Nanni, Daniele; Navacchia, Maria Luisa
Tetrahedron, 1996 , vol. 52, # 41 p. 13255 - 13264
反应条件
1: Et3N / CH2Cl2 / 3 h / 0 °C
2: 1.) LDA, 2.) O2 / 1.) THF, RT, 4 h, 2.) THF, RT, 20 h
View Scheme
参考文献
Barbieri, Anna; Montevecchi, Pier Carlo; Nanni, Daniele; Navacchia, Maria Luisa
Tetrahedron, 1996 , vol. 52, # 41 p. 13255 - 13264
