5-溴-N-(叔丁氧羰基)吲哚2-硼酸合成路线 （共 3 条）
反应条件
1: With tri-isopropoxy-borane; lithium diisopropyl amide in tetrahydrofuran T=0 - 5°C; 0.5 h; 2: With hydrogenchloride in tetrahydrofuran Further stages.;
参考文献
Vazquez, Enrique; Davies, Ian W.; Payack, Joseph F.
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7551 - 7552
反应条件
1.1: DMAP / CH2Cl2 / 0.75 h / 20 °C 2.1: (iPrO)3B; LDA / tetrahydrofuran / 0.5 h / 0 - 5 °C 2.2: 92 percent Chromat. / 2N HCl / tetrahydrofuran View Scheme
参考文献
Vazquez, Enrique; Davies, Ian W.; Payack, Joseph F.
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7551 - 7552
反应条件
1.1: DMAP / CH2Cl2 / 0.75 h / 20 °C 2.1: (iPrO)3B; LDA / tetrahydrofuran / 0.5 h / 0 - 5 °C 2.2: 92 percent Chromat. / 2N HCl / tetrahydrofuran View Scheme
参考文献
Vazquez, Enrique; Davies, Ian W.; Payack, Joseph F.
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7551 - 7552
