1-Boc-2-(羟基二甲基锡)-5-甲基吲哚合成路线 （共 3 条）
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran
T=0 - 5°C; 0.5 h;
2: With sodium hydrogencarbonate
1 h; Further stages.;
参考文献
Vazquez, Enrique; Davies, Ian W.; Payack, Joseph F.
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7551 - 7552
反应条件
1.1: DMAP / CH2Cl2 / 0.75 h / 20 °C
2.1: LDA / tetrahydrofuran / 0.5 h / 0 - 5 °C
2.2: 91 percent / aq. NaHCO3 / 1 h
View Scheme
参考文献
Vazquez, Enrique; Davies, Ian W.; Payack, Joseph F.
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7551 - 7552
反应条件
1.1: DMAP / CH2Cl2 / 0.75 h / 20 °C
2.1: LDA / tetrahydrofuran / 0.5 h / 0 - 5 °C
2.2: 91 percent / aq. NaHCO3 / 1 h
View Scheme
参考文献
Vazquez, Enrique; Davies, Ian W.; Payack, Joseph F.
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7551 - 7552
