4-甲氧基苄基硼酸频哪醇酯合成路线 （共 11 条）
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=20°C; Suzuki-Miyaura Coupling; 2 h; Time; chemoselective reaction;
参考文献
Endo, Kohei; Kurosawa, Fumiya; Ukaji, Yutaka
Chemistry Letters, 2013 , vol. 42, # 11 p. 1363 - 1365
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in 1,4-dioxane T=100°C; Suzuki cross-coupling reaction; 18 h;
参考文献
Giroux, Andre
Tetrahedron Letters, 2003 , vol. 44, # 2 p. 233 - 235
反应条件
lithium bis((trifluoromethyl)sulfonyl)amide in tetrahydrofuran T=20°C; Electrochemical reaction;
参考文献
Pintaric; Laza; Olivero; Dunach
Tetrahedron Letters, 2004 , vol. 45, # 43 p. 8031 - 8033
反应条件
magnesium; triethylamine in tetrahydrofuran Barbier-type reaction; 15 h; Inert atmosphereReflux;
参考文献
Pintaric, Christine; Olivero, Sandra; Gimbert, Yves; Chavant, Pierre Y.; Dunach, Elisabet
Journal of the American Chemical Society, 2010 , vol. 132, # 34 p. 11825 - 11827
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=50°C; Alkylation; 7 h;
参考文献
Falck; Bondlela, Muralidhar; Ye, Jianhua; Su-Dong, Cho
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5647 - 5650
反应条件
bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine in 1,2-dichloro-ethane T=80°C; 6 h;
参考文献
Murata, Miki; Oyama, Takashi; Watanabe, Shinji; Masuda, Yuzuru
Synthetic Communications, 2002 , vol. 32, # 16 p. 2513 - 2517
反应条件
sodium methylate in methanol; toluene T=90°C; Inert atmosphere;
参考文献
Li, Huan; Wang, Long; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 12 p. 2943 - 2946
反应条件
palladium on activated charcoal in not given byproducts: H2; 16 h or more at 100°C under N2; catalyst: 10percent Pd/C (6 molpercent or more);
参考文献
Ishiyama, Tatsuo; Ishida, Kousaku; Takagi, Jun; Miyaura, Norio
Chemistry Letters, 2001 , # 11 p. 1082 - 1083
反应条件
1: methanol / 70 °C / Inert atmosphere 2: sodium methylate / methanol; toluene / 90 °C / Inert atmosphere View Scheme
参考文献
Li, Huan; Wang, Long; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 12 p. 2943 - 2946
反应条件
NaOMe in methanol; toluene 90°C, 3-12 h;
参考文献
Li, Huan; Wang, Long; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 12 p. 2943 - 2946
