3-(对枯烯基)-2-甲基丙醇合成路线 （共 12 条）
反应条件
Dess-Martin periodane 1 h;
参考文献
RSC Advances, , vol. 3, # 14 p. 4496 - 4499
反应条件
zirconium oxide in isopropyl alcohol
5 h; Heating;
参考文献
Matsushita, Hajime; Ishiguro, Shigeo; Ichinose, Hiroshi; Izumi, Akira; Mizusaki, Shigenobu
Chemistry Letters, 1985 , p. 731 - 734
反应条件
5 palladium on charcoal; hydrogen in methanol
24 h;
参考文献
Limnios, Dimitris; Kokotos, Christoforos G.
RSC Advances, 2013 , vol. 3, # 14 p. 4496 - 4499
反应条件
hydrogen; Rh/Al2O3 in ethanol; water
T=59.9°C; P=750.06 Torr; influence of various (Ni, Pd, Rh) catalysts at different temperatures; selectivity of the reaction; dependence of the hydrogenation rate on the amount of hydrogen absorbed, and the hydrogen pressure; Product distributionRate constant;
参考文献
Pak; Konuspaev; Sagindykov; Sokol'skii; Zapletal; Prykhlik
Journal of applied chemistry of the USSR, 1986 , vol. 59, # 5 pt 2 p. 1058 - 1060
反应条件
hydrogen; sodium carbonate; Catalyst M-Chromium oxide; nickel in ethanol; water
T=110°C; P=22800 Torr; other temperature, other solvent, other pressure, other catalysts; Product distribution;
参考文献
Sokol'skii, D. V.; Pak, A. M.; Turganbaeva, S. M.; Konuspaev, S. R.; Ginzburg, M. A.
J. Appl. Chem. USSR (Engl. Transl.), 1981 , vol. 54, # 7 p. 1574 - 1578,1345 - 1347
反应条件
1: pyrrolidine / neat (no solvent) / 0.25 h / 120 °C / |Microwave irradiation
2: hydrogen; 5 palladium on charcoal / methanol / 24 h
View Scheme
参考文献
Limnios, Dimitris; Kokotos, Christoforos G.
RSC Advances, 2013 , vol. 3, # 14 p. 4496 - 4499
反应条件
2,6-dimethylheptan-4-ol; sodium; xylene
参考文献
Beets; van Essen
Recueil des Travaux Chimiques des Pays-Bas, 1951 , vol. 70, p. 25,27
反应条件
ethanol; nickel
Hydrogenation;
参考文献
Shinya
Nippon Nogei Kagaku Kaishi, 1959 , vol. 33, p. 261,265
反应条件
1: aqueous KOH
2: water; sulfuric acid
3: 2,6-dimethyl-heptan-4-ol; sodium; xylene
View Scheme
参考文献
Beets; van Essen
Recueil des Travaux Chimiques des Pays-Bas, 1951 , vol. 70, p. 25,27
反应条件
1: NaBH4
2: Raney nickel; ethanol / Hydrogenation
View Scheme
参考文献
Shinya
Nippon Nogei Kagaku Kaishi, 1959 , vol. 33, p. 261,265
