2-甲基-3-苯基-1H-吲哚合成路线 （共 49 条）
反应条件
lithium vanadium(I) dihydride in tetrahydrofuran
T=25°C; 12 h; Inert atmosphere;
参考文献
Eisch, John J.; Fregene, Paul O.
European Journal of Organic Chemistry, 2008 , # 26 p. 4482 - 4492
反应条件
Ti/C in tetrahydrofuran
参考文献
Fuerstner, Alois; Jumbam, Denis N.
Tetrahedron, 1992 , vol. 48, # 29 p. 5991 - 6010
反应条件
phosphorus trichoride in dichloromethane
0.5 h; Ambient temperature;
参考文献
Baccolini, Grazieno; Dalpozzo, Renato; Todesco, Paolo E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 971 - 974
反应条件
triethyl phosphite
T=150°C; 2 h;
参考文献
Russell, Glen A.; Yao, Ching-Fa
Journal of Organic Chemistry, 1992 , vol. 57, # 24 p. 6508 - 6513
反应条件
Lawesson's reagent in benzene
T=80°C; 4 h;
参考文献
El-Barbary, A. A.; Lawesson, S.-O.
Tetrahedron, 1981 , vol. 37, # 15 p. 2647 - 2650
反应条件
caesium carbonate; bis(dibenzylideneacetone)-palladium(0) in toluene
T=150°C; 24 h; Inert atmosphere;
参考文献
Tan, Yichen; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3676 - 3677
反应条件
1: NaOAc; NH2OH*HCl / methanol; H2O / 4 h / 20 °C
2: 75 mg / DIAD; tri-n-butylphosphine / acetonitrile / 2 h / 20 °C
3: 89 percent / o-xylene / 16 h / 150 °C
View Scheme
参考文献
Taber, Douglass F.; Tian, Weiwei
Journal of the American Chemical Society, 2006 , vol. 128, # 4 p. 1058 - 1059
反应条件
1: With potassium carbonate in 1,4-dioxane
T=100°C; 8 h;
2: With copper(l) iodide in 1,4-dioxane
T=20 - 120°C; 5 h;
参考文献
Wang, Xianxue; Liu, Jin; Guo, Han; Ma, Chao; Gao, Xiai; Zhou, Kang; Huang, Guosheng
Synthesis, 2012 , vol. 44, # 7 p. 1037 - 1042
反应条件
acetic acid
T=100°C; Fischer reaction; 3 h;
参考文献
Rodriguez; Lafuente; Garcia-Almaraz
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 5 p. 1281 - 1288
反应条件
samarium diiodide in tetrahydrofuran
T=65°C; 1 h;
参考文献
Fan, Xuesen; Zhang, Yongmin
Tetrahedron, 2003 , vol. 59, # 11 p. 1917 - 1923
