2-甲基-3-苯基-1H-吲哚合成路线 (共 49 条)
反应条件
1: benzene / Heating
2: H2 / 10percent Pd/C / benzene / 20 °C
View Scheme
参考文献
Penoni, Andrea; Volkmann, Jerome; Nicholas, Kenneth M.
Organic Letters, 2002 , vol. 4, # 5 p. 699 - 701
反应条件
1: benzene / Heating
2: H2 / 10percent Pd/C / benzene / 20 °C
View Scheme
参考文献
Penoni, Andrea; Volkmann, Jerome; Nicholas, Kenneth M.
Organic Letters, 2002 , vol. 4, # 5 p. 699 - 701
反应条件
1: 75 mg / DIAD; tri-n-butylphosphine / acetonitrile / 2 h / 20 °C
2: 89 percent / o-xylene / 16 h / 150 °C
View Scheme
参考文献
Taber, Douglass F.; Tian, Weiwei
Journal of the American Chemical Society, 2006 , vol. 128, # 4 p. 1058 - 1059
反应条件
phosphorus trichoride in benzene
Ambient temperature;
参考文献
Baccolini, Graziano; Todesco, Paolo E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 3 p. 535 - 538
反应条件
1: 78 percent / NaH / dimethylformamide / 1 h / 0 °C
2: 85 percent / Rh2(OCOCF3)4 / 1,2-dichloro-ethane / 1 h / 60 °C
View Scheme
参考文献
Chiba, Shunsuke; Hattori, Gaku; Narasaka, Koichi
Chemistry Letters, 2007 , vol. 36, # 1 p. 52 - 53
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
Reduction; 14 h; Heating;
参考文献
Bruni, Paolo; Giorgini, Elisabetta; Tommasi, Giampaolo; Greci, Lucedio
Tetrahedron, 1998 , vol. 54, # 20 p. 5305 - 5314
反应条件
potassium carbonate; [Pd(NH3)4](2+)/NaY zeolite in 1,4-dioxane
Heating;
参考文献
Cusati, Giuseppe; Djakovitch, Laurent
Tetrahedron Letters, 2008 , vol. 49, # 16 p. 2499 - 2502
反应条件
Fe pythalocyanine in toluene
RefluxInert atmosphere; regioselective reaction;
参考文献
Lamar, Angus A.; Nicholas, Kenneth M.
Tetrahedron, 2009 , vol. 65, # 19 p. 3829 - 3833
反应条件
1: With [Pd(P{(C6H11)3})2] in toluene
T=20°C;
2: With caesium carbonate in toluene
T=150°C; 2 h;
参考文献
Tan, Yichen; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3676 - 3677
反应条件
copper in dichloromethane
18 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Finet, Jean-Pierre; Khamsi, Jamal
Tetrahedron Letters, 1988 , vol. 29, # 10 p. 1115 - 1118