2-甲基-3-苯基-1H-吲哚合成路线 （共 49 条）
反应条件
1: 78 percent / pyridine / CH2Cl2 / Ambient temperature
2: 87 percent / Ti-graphite / tetrahydrofuran / Heating
View Scheme
参考文献
Fuerstner, Alois; Jumbam, Denis N.
Tetrahedron, 1992 , vol. 48, # 29 p. 5991 - 6010
反应条件
1: toluenesulfonyl azide
2: decahydronaphthalene / 2 h / 195 °C
View Scheme
参考文献
Smith, P. A. S.; Rowe, C. D.r.; Hansen, D. W. Jr.
Tetrahedron Letters, 1983 , vol. 24, # 47 p. 5169 - 5172
反应条件
1: 28 percent
2: toluenesulfonyl azide
3: decahydronaphthalene / 2 h / 195 °C
View Scheme
参考文献
Smith, P. A. S.; Rowe, C. D.r.; Hansen, D. W. Jr.
Tetrahedron Letters, 1983 , vol. 24, # 47 p. 5169 - 5172
反应条件
1: 1-methyl-pyrrolidin-2-one; copper(l) iodide; dichloro bis(acetonitrile) palladium(II); triphenyl-arsane / 72 h / 80 °C / Inert atmosphere
2: carbon monoxide; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 72 h / 120 °C / 4560.31 Torr / Autoclave
View Scheme
参考文献
Banini, Serge R.; Turner, Michael R.; Cummings, Matthew M.; Soederberg, Bjoern C.G.
Tetrahedron, 2011 , vol. 67, # 20 p. 3603 - 3611
反应条件
1: 1-methyl-pyrrolidin-2-one; copper(l) iodide; dichloro bis(acetonitrile) palladium(II); triphenyl-arsane / 72 h / 80 °C / Inert atmosphere
2: carbon monoxide; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 72 h / 120 °C / 4560.31 Torr / Autoclave
View Scheme
参考文献
Banini, Serge R.; Turner, Michael R.; Cummings, Matthew M.; Soederberg, Bjoern C.G.
Tetrahedron, 2011 , vol. 67, # 20 p. 3603 - 3611
反应条件
aluminium trichloride; 1-butylpyridinium chloride
Fischer indole synthesis; 0.666667 h; Heating;
参考文献
Rebeiro; Khadilkar
Synthesis, 2001 , # 3 p. 370 - 372
反应条件
hydrogenchloride in ethanol
2 h; Ambient temperature; Yield given;
参考文献
Berti, Corrado; Greci, Lucedio; Poloni, Marino
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1610 - 1613
反应条件
1: 13 h / 40 °C
2: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C
3: Ni(cyclooctadiene)2; tricyclopentyl-phosphine / toluene / 12 h / 80 °C
View Scheme
参考文献
Okamoto, Kazuhiro; Mashida, Ayano; Watanabe, Masahito; Ohe, Kouichi
Chemical Communications, 2012 , vol. 48, # 29 p. 3554 - 3556
反应条件
in benzene
T=80°C; 4 h; Mechanism;
参考文献
El-Barbary, A. A.; Lawesson, S.-O.
Tetrahedron, 1981 , vol. 37, # 15 p. 2647 - 2650
反应条件
T=150°C; 2 h; various 1-nitro-2,2-diphenylethylenes and β-nitrostyrenes; other conditions; Product distributionMechanism;
参考文献
Russell, Glen A.; Yao, Ching-Fa
Journal of Organic Chemistry, 1992 , vol. 57, # 24 p. 6508 - 6513
