N-甲基-1,2-苯二胺合成路线 （共 142 条）
反应条件
1: N-methyl-para-phenylenediamine With trimethylaluminum chloride in toluene
T=0 - 20°C;
2: hydroxymethyl JandaJelTM resin-bound styryl ester in toluene
24 h; Heating; Further stages.;
参考文献
Matsushita, Hana; Lee, Sang-Hyeup; Joung, Meyoungju; Clapham, Bruce; Janda, Kim D.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 313 - 316
反应条件
hydrogenchloride; manganese(IV) oxide; 4 A molecular sieve in diethyl ether; toluene
T=105°C; 18 h;
参考文献
Wilfred, Cecilia D.; Taylor, Richard J. K.
Synlett, 2004 , # 9 p. 1628 - 1630
反应条件
H4SiW12O40 in ethyl acetate
T=20°C; 0.0833333 h;
参考文献
Chakrabarty, Manas; Mukherji, Ajanta; Mukherjee, Ratna; Arima, Shiho; Harigaya, Yoshihiro
Tetrahedron Letters, 2007 , vol. 48, # 30 p. 5239 - 5242
反应条件
1: 85 percent / methanol / 0.08 h / Ambient temperature
2: 92 percent / methanol / 6 h / Ambient temperature
3: 97 percent / benzylidenemalonitrile / ethanol / 12 h / Ambient temperature
View Scheme
参考文献
Hawkins, David; Lindley, John M.; McRobbie, Ian M.; Meth-Cohn, Otto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2387 - 2391
参考文献
Cappel; Fernelius
Journal of Organic Chemistry, 1940 , vol. 5, p. 40,44
参考文献
Rene, Olivier; Souverneva, Alexandra; Magnuson, Steven R.; Fauber, Benjamin P.
Tetrahedron Letters, 2013 , vol. 54, # 3 p. 201 - 204
反应条件
aluminum oxide
T=110 - 120°C; 0.0666667 h; microwave irradiation;
参考文献
Chauhan; Singh, Ram; Geetanjali
Synthetic Communications, 2003 , vol. 33, # 7 p. 1179 - 1184
参考文献
Kuhn; Weygand
Chemische Berichte, 1934 , vol. 67, p. 1459
参考文献
Schipper; Day
Journal of the American Chemical Society, 1951 , vol. 73, p. 5672,5673
反应条件
sodium hydride in toluene; mineral oil
T=150°C; 16 h;
参考文献
Sluiter, Jonas; Christoffers, Jens
Synlett, 2009 , # 1 p. 63 - 66
