N-甲基-1,2-苯二胺合成路线 (共 142 条)
参考文献
Hempel
Journal fuer Praktische Chemie (Leipzig), 1890 , vol. <2>41, p. 164
参考文献
Hempel
Journal fuer Praktische Chemie (Leipzig), 1890 , vol. <2>41, p. 164
反应条件
2: hydrazine View Scheme
参考文献
Armand; Boulares; et al.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 6 p. 1519 - 1525
反应条件
polyphosphoric acid T=210°C; 4 h; Neat (no solvent);
参考文献
Yang, Wen-Wen; Zhong, Yu-Wu; Yoshikawa, Shinpei; Shao, Jiang-Yang; Masaoka, Shigeyuki; Sakai, Ken; Yao, Jiannian; Haga, Masa-Aki
Inorganic Chemistry, 2012 , vol. 51, # 2 p. 890 - 899
反应条件
1: With hydrogenchloride in water T=55°C; 2: With water; sodium hydrogencarbonate
参考文献
PLEXXIKON, INC.
Patent: WO2008/80001 A2, 2008 ;
Location in patent: Page/Page column 105-106 ;
反应条件
in dichloromethane Ambient temperature;
参考文献
Musser; Kubrak; Chang; DiZio; Hite; Hand; Lewis
Journal of medicinal chemistry, 1987 , vol. 30, # 2 p. 400 - 405
反应条件
1: 140 - 150 °C 2: SOCl2 View Scheme
参考文献
Mamalis et al.
Journal of the Chemical Society, 1950 , p. 1600,1602
反应条件
triphenyl phosphite in pyridine T=220°C; 0.166667 h; microwave irradiation;
参考文献
Lin, Shou-Yuan; Isome, Yuko; Stewart, Ethan; Liu, Ji-Feng; Yohannes, Daniel; Yu, Libing
Tetrahedron Letters, 2006 , vol. 47, # 17 p. 2883 - 2886
反应条件
Pt-TiO2 T=32°C; 4 h; UV-irradiationInert atmosphere;
参考文献
Selvam; Swaminathan
Tetrahedron Letters, 2011 , vol. 52, # 26 p. 3386 - 3392
反应条件
1: 77.2 percent / ethanol / 50 °C 2: 49 percent / N-bromosuccinimide; benzoyl peroxide / CCl4 / 10.5 h / Heating View Scheme
参考文献
Lawrence; Copper; Smith
Journal of Medicinal Chemistry, 2001 , vol. 44, # 4 p. 594 - 601