N-甲基-1,2-苯二胺合成路线 （共 142 条）
反应条件
oxygen; 1-hexadecylpyridinium bromide in water T=20°C; 0.75 h;
参考文献
Chakrabarty, Manas; Karmakar, Sulakshana; Mukherjee, Ratna; Arima, Shiho; Harigaya, Yoshihiro
Monatshefte fur Chemie, 2009 , vol. 140, # 4 p. 375 - 380
反应条件
hydrogenchloride; manganese(IV) oxide; 4 A molecular sieve in diethyl ether; toluene T=105°C; 18 h;
参考文献
Wilfred, Cecilia D.; Taylor, Richard J. K.
Synlett, 2004 , # 9 p. 1628 - 1630
反应条件
sodium hydride in toluene; mineral oil T=150°C; 16 h;
参考文献
Sluiter, Jonas; Christoffers, Jens
Synlett, 2009 , # 1 p. 63 - 66
参考文献
McKinnon, David M.; Spevack, Perry; Tipples, Graham
Canadian Journal of Chemistry, 1988 , vol. 66, p. 2339 - 2344
反应条件
palladium 10 on activated carbon in N-dodecane; N,N-dimethyl acetamide T=120°C; 14 h; Inert atmosphere;
参考文献
Jin, Xukang; Liu, Yuxiao; Lu, Qiongqiong; Yang, Dejun; Sun, Jiangkai; Qin, Shuangshuang; Zhang, Jingwu; Shen, Jiaxuan; Chu, Changhu; Liu, Renhua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3776 - 3780
反应条件
palladium 10 on activated carbon in N-dodecane; N,N-dimethyl acetamide T=120°C; 24 h; Inert atmosphere;
参考文献
Jin, Xukang; Liu, Yuxiao; Lu, Qiongqiong; Yang, Dejun; Sun, Jiangkai; Qin, Shuangshuang; Zhang, Jingwu; Shen, Jiaxuan; Chu, Changhu; Liu, Renhua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3776 - 3780
反应条件
1: N-methyl-para-phenylenediamine With trimethylaluminum chloride in toluene T=0 - 20°C; 2: hydroxymethyl JandaJelTM resin-bound 4-MeOPh ester in toluene 24 h; Heating; Further stages.;
参考文献
Matsushita, Hana; Lee, Sang-Hyeup; Joung, Meyoungju; Clapham, Bruce; Janda, Kim D.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 313 - 316
反应条件
hydrogenchloride; manganese(IV) oxide; 4 A molecular sieve in diethyl ether; toluene T=105°C; 18 h;
参考文献
Wilfred, Cecilia D.; Taylor, Richard J. K.
Synlett, 2004 , # 9 p. 1628 - 1630
反应条件
sodium hydride in toluene; mineral oil T=180°C; 6 h;
参考文献
Sluiter, Jonas; Christoffers, Jens
Synlett, 2009 , # 1 p. 63 - 66
参考文献
Journal of the Chemical Society, , p. 2296
