反应条件
1: hydroquinine 1,4-phthalazinediyl diether; K3Fe(CN)6; K2OsO4*2H2O / K2CO3; methanesulfonamide / H2O; 2-methyl-propan-2-ol / 168 h / 4 °C 2: 60 mg / p-toluenesulfonic acid / CH2Cl2 / 3 h / 20 °C 3: 100 percent / H2; palladium(II) chloride / methanol / 0.5 h / 20 °C 4: 94.3 percent / hydrochloric acid / H2O; tetrahydrofuran / 20 h / 20 °C View Scheme
参考文献
Lindsay, Karl B.; Pyne, Stephen G.
Journal of Organic Chemistry, 2002 , vol. 67, # 22 p. 7774 - 7780
