titanium tetrachloride; zinc in tetrahydrofuran T=-20 - -10°C; McMurry reaction; 4 h; Inert atmosphere; optical yield given as percent de;
参考文献
Abad, Andres; Lopez-Perez, Jose L.; Del Olmo, Esther; Garcia-Fernandez, Luis F.; Francesch, Andres; Trigili, Chiara; Barasoain, Isabel; Andreu, Jose M.; Fernand Diaz; San Feliciano, Arturo
Journal of Medicinal Chemistry, 2012 , vol. 55, # 15 p. 6724 - 6737
Abad, Andres; Lopez-Perez, Jose L.; Del Olmo, Esther; Garcia-Fernandez, Luis F.; Francesch, Andres; Trigili, Chiara; Barasoain, Isabel; Andreu, Jose M.; Fernand Diaz; San Feliciano, Arturo
Journal of Medicinal Chemistry, 2012 , vol. 55, # 15 p. 6724 - 6737
Abad, Andres; Lopez-Perez, Jose L.; Del Olmo, Esther; Garcia-Fernandez, Luis F.; Francesch, Andres; Trigili, Chiara; Barasoain, Isabel; Andreu, Jose M.; Fernand Diaz; San Feliciano, Arturo
Journal of Medicinal Chemistry, 2012 , vol. 55, # 15 p. 6724 - 6737
Abad, Andres; Lopez-Perez, Jose L.; Del Olmo, Esther; Garcia-Fernandez, Luis F.; Francesch, Andres; Trigili, Chiara; Barasoain, Isabel; Andreu, Jose M.; Fernand Diaz; San Feliciano, Arturo
Journal of Medicinal Chemistry, 2012 , vol. 55, # 15 p. 6724 - 6737
titanium tetrachloride; zinc in tetrahydrofuran T=-20 - -10°C; McMurry reaction; 4 h; Inert atmosphere; optical yield given as percent de;
参考文献
Abad, Andres; Lopez-Perez, Jose L.; Del Olmo, Esther; Garcia-Fernandez, Luis F.; Francesch, Andres; Trigili, Chiara; Barasoain, Isabel; Andreu, Jose M.; Fernand Diaz; San Feliciano, Arturo
Journal of Medicinal Chemistry, 2012 , vol. 55, # 15 p. 6724 - 6737
Abad, Andres; Lopez-Perez, Jose L.; Del Olmo, Esther; Garcia-Fernandez, Luis F.; Francesch, Andres; Trigili, Chiara; Barasoain, Isabel; Andreu, Jose M.; Fernand Diaz; San Feliciano, Arturo
Journal of Medicinal Chemistry, 2012 , vol. 55, # 15 p. 6724 - 6737
1: acetaldehyde; (-)-podophyllotoxon With titanium tetrachloride; zinc in tetrahydrofuran T=-20 - -10°C; McMurry reaction; 4 h; Inert atmosphere; 2: 2,2-dimethoxy-propane With chloro-trimethyl-silane in acetone 0.0833333 h; Inert atmosphere;
参考文献
Abad, Andres; Lopez-Perez, Jose L.; Del Olmo, Esther; Garcia-Fernandez, Luis F.; Francesch, Andres; Trigili, Chiara; Barasoain, Isabel; Andreu, Jose M.; Fernand Diaz; San Feliciano, Arturo
Journal of Medicinal Chemistry, 2012 , vol. 55, # 15 p. 6724 - 6737