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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
丹宁卡
合成路线
（共 14 条）
1401311-38-3
→
反应条件
477-84-9
丹宁卡
反应条件
1: With N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 24 h; Reflux; 2: With acetic acid in water 24 h; Reflux;
参考文献
Saha, Koushik; Lam, Kok Wai; Abas, Faridah; Sazali Hamzah; Stanslas, Johnson; Hui, Lim Siang; Lajis, Nordin H.
Medicinal Chemistry Research, 2013 , vol. 22, # 5 p. 2093 - 2104
85-44-9
苯酐
→
反应条件
477-84-9
丹宁卡
反应条件
1.1: AlCl3, aluminium chloride; sodium chloride / 0.75 h / 165 - 170 °C 2.1: potassium carbonate / acetone / 20 h / 20 °C 3.1: potassium carbonate / acetone / 22 h / |Reflux 4.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 5.1: sodium hydroxide / water / 24 h / 20 °C 6.1: potassium carbonate / acetone / 20 h / 20 °C 7.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 7.2: 24 h / |Reflux View Scheme
参考文献
Akhtar, Muhammad Nadeem; Zareen, Seema; Yeap, Swee Keong; Ho, Wan Yong; Lo, Kong Mun; Hasan, Aurangzeb; Alitheen, Noorjahan Banu
Molecules, 2013 , vol. 18, # 8 p. 10042 - 10055
117-02-2
茜根定
→
反应条件
477-84-9
丹宁卡
反应条件
1.1: potassium carbonate / acetone / 20 h / 20 °C 2.1: potassium carbonate / acetone / 22 h / |Reflux 3.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 4.1: sodium hydroxide / water / 24 h / 20 °C 5.1: potassium carbonate / acetone / 20 h / 20 °C 6.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 6.2: 24 h / |Reflux View Scheme
参考文献
Akhtar, Muhammad Nadeem; Zareen, Seema; Yeap, Swee Keong; Ho, Wan Yong; Lo, Kong Mun; Hasan, Aurangzeb; Alitheen, Noorjahan Banu
Molecules, 2013 , vol. 18, # 8 p. 10042 - 10055
10383-64-9
→
反应条件
477-84-9
丹宁卡
反应条件
1.1: potassium carbonate / acetone / 22 h / |Reflux 2.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 3.1: sodium hydroxide / water / 24 h / 20 °C 4.1: potassium carbonate / acetone / 20 h / 20 °C 5.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 5.2: 24 h / |Reflux View Scheme
参考文献
Akhtar, Muhammad Nadeem; Zareen, Seema; Yeap, Swee Keong; Ho, Wan Yong; Lo, Kong Mun; Hasan, Aurangzeb; Alitheen, Noorjahan Banu
Molecules, 2013 , vol. 18, # 8 p. 10042 - 10055
2324-25-6
→
反应条件
477-84-9
丹宁卡
反应条件
1.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 2.1: sodium hydroxide / water / 24 h / 20 °C 3.1: potassium carbonate / acetone / 20 h / 20 °C 4.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 4.2: 24 h / |Reflux View Scheme
参考文献
Akhtar, Muhammad Nadeem; Zareen, Seema; Yeap, Swee Keong; Ho, Wan Yong; Lo, Kong Mun; Hasan, Aurangzeb; Alitheen, Noorjahan Banu
Molecules, 2013 , vol. 18, # 8 p. 10042 - 10055
63965-55-9
→
反应条件
477-84-9
丹宁卡
反应条件
1.1: sodium hydroxide / water / 24 h / 20 °C 2.1: potassium carbonate / acetone / 20 h / 20 °C 3.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 3.2: 24 h / |Reflux View Scheme
参考文献
Akhtar, Muhammad Nadeem; Zareen, Seema; Yeap, Swee Keong; Ho, Wan Yong; Lo, Kong Mun; Hasan, Aurangzeb; Alitheen, Noorjahan Banu
Molecules, 2013 , vol. 18, # 8 p. 10042 - 10055
63965-57-1
→
反应条件
477-84-9
丹宁卡
反应条件
1.1: potassium carbonate / acetone / 20 h / 20 °C 2.1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 24 h / |Reflux 2.2: 24 h / |Reflux View Scheme
参考文献
Akhtar, Muhammad Nadeem; Zareen, Seema; Yeap, Swee Keong; Ho, Wan Yong; Lo, Kong Mun; Hasan, Aurangzeb; Alitheen, Noorjahan Banu
Molecules, 2013 , vol. 18, # 8 p. 10042 - 10055
477-83-8
虎刺醇
→
反应条件
477-84-9
丹宁卡
反应条件
manganese(IV) oxide
参考文献
Hirose
Yakugaku Zasshi, 1956 , vol. 76, p. 1448
Chemical and Pharmaceutical Bulletin, 1960 , vol. 8, p. 417,422
Full Text Show Details
Ayyangar et al.
Tetrahedron, 1959 , vol. 6, p. 331,335
478-08-0
1,3-二羟基-2-(羟基甲基)蒽醌
→
反应条件
477-84-9
丹宁卡
反应条件
1: triacetyl borate 2: 1,1,2,2-tetrachloro-ethane; diethyl ether 3: methanol. KOH 4: MnO2 View Scheme
参考文献
Ayyangar et al.
Tetrahedron, 1959 , vol. 6, p. 331,335
63965-56-0
→
反应条件
477-84-9
丹宁卡
反应条件
1: methanol. KOH 2: MnO2 View Scheme
参考文献
Ayyangar et al.
Tetrahedron, 1959 , vol. 6, p. 331,335
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