1,2,3-三甲基-1H-茚合成路线 （共 10 条）
反应条件
toluene-4-sulfonic acid in toluene
Dehydration; 5 h; Heating;
参考文献
Ready, Thomas E.; Chien, James C.W.; Rausch, Marvin D.
Journal of Organometallic Chemistry, 1999 , vol. 583, # 1-2 p. 11 - 27
反应条件
1: 84 percent / AlCl3 / Heating
2: 86 percent / diethyl ether / Heating
3: 79 percent / p-TsOH / toluene / 5 h / Heating
View Scheme
参考文献
Ready, Thomas E.; Chien, James C.W.; Rausch, Marvin D.
Journal of Organometallic Chemistry, 1999 , vol. 583, # 1-2 p. 11 - 27
反应条件
1: thionyl chloride / 15 h / Heating
2: 84 percent / AlCl3 / Heating
3: 86 percent / diethyl ether / Heating
4: 79 percent / p-TsOH / toluene / 5 h / Heating
View Scheme
参考文献
Ready, Thomas E.; Chien, James C.W.; Rausch, Marvin D.
Journal of Organometallic Chemistry, 1999 , vol. 583, # 1-2 p. 11 - 27
参考文献
Miller,W.G.; Pittman,C.V.
Journal of Organic Chemistry, 1974 , vol. 39, # 13 p. 1955 - 1956
反应条件
aluminium trichloride
参考文献
Skattebol,L.; Boulette,B.
Journal of Organic Chemistry, 1966 , vol. 31, p. 81 - 85
反应条件
1: AlCl3
2: (i) , (ii) (heating), H2SO4
View Scheme
参考文献
Gelin,R.; Chantegrel,B.
Bulletin de la Societe Chimique de France, 1971 , p. 2527 - 2544
反应条件
aluminium trichloride
参考文献
Buddrus,J.
Chemische Berichte, 1968 , vol. 101, p. 4152 - 4162
反应条件
(i) , (ii) (heating), H2SO4; Multistep reaction;
参考文献
Gelin,R.; Chantegrel,B.
Bulletin de la Societe Chimique de France, 1971 , p. 2527 - 2544
参考文献
Plattner; Fuerst; Jirasek
Helvetica Chimica Acta, 1947 , vol. 30, p. 1320,1328
反应条件
1: oxirane, <Et4N>Br
2: H2, NaOH / Pd-C / methanol
View Scheme
参考文献
Buddrus,J.
Chemische Berichte, 1968 , vol. 101, p. 4152 - 4162
