4-羟基-6,8-二甲氧基-2-萘羧酸乙酯合成路线 （共 4 条）
反应条件
acetyl chloride in methanol
T=0 - 20°C; 12 h;
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470
反应条件
1: t-BuOK / 2-methyl-propan-2-ol / 2 h / Heating
2: 8.10 g / sodium acetate / 2 h / 140 °C
3: 95 percent / guanidine hydrochloride; t-BuOK / ethanol; CH2Cl2 / 1.5 h / 20 °C
View Scheme
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470
反应条件
1: 8.10 g / sodium acetate / 2 h / 140 °C
2: 95 percent / guanidine hydrochloride; t-BuOK / ethanol; CH2Cl2 / 1.5 h / 20 °C
View Scheme
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470
反应条件
potassium carbonate in acetone
16 h; Heating;
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470
