6,8-二甲氧基-4-(2-丙烯-1-基氧基)-2-萘羧酸乙酯合成路线 (共 4 条)
反应条件
potassium carbonate in acetone
16 h; Heating;
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470
反应条件
1: 95 percent / guanidine hydrochloride; t-BuOK / ethanol; CH2Cl2 / 1.5 h / 20 °C
2: 99 percent / K2CO3 / acetone / 16 h / Heating
View Scheme
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470
反应条件
1: t-BuOK / 2-methyl-propan-2-ol / 2 h / Heating
2: 8.10 g / sodium acetate / 2 h / 140 °C
3: 95 percent / guanidine hydrochloride; t-BuOK / ethanol; CH2Cl2 / 1.5 h / 20 °C
4: 99 percent / K2CO3 / acetone / 16 h / Heating
View Scheme
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470
反应条件
1: 8.10 g / sodium acetate / 2 h / 140 °C
2: 95 percent / guanidine hydrochloride; t-BuOK / ethanol; CH2Cl2 / 1.5 h / 20 °C
3: 99 percent / K2CO3 / acetone / 16 h / Heating
View Scheme
参考文献
Mmutlane, Edwin M.; Michael, Joseph P.; Green, Ivan R.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2461 - 2470