Cbz-L-天冬氨酸-Alpha苄脂合成路线 (共 22 条)
反应条件
triethylamine in dichloromethane T=0°C; 1 h; Yield given. Title compound not separated from byproducts;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
反应条件
triethylamine in dichloromethane T=0°C; 1 h; Yields of byproduct given;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
反应条件
in tetrahydrofuran T=20°C; Substitution;
参考文献
Wiemann, Arndt; Frank, Ronald; Tegge, Werner
Tetrahedron, 2000 , vol. 56, # 10 p. 1331 - 1337
参考文献
Furuta, Takashi; Katayama, Motofusa; Shibasaki, Hiromi; Kasuya, Yasuji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1643 - 1648
反应条件
4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=0 - 20°C; 20 h; Title compound not separated from byproducts.;
参考文献
Burtin, Guillaume; Corringer, Pierre-Jean; Young, Douglas W.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 20 p. 3451 - 3459
反应条件
in tetrahydrofuran T=20°C; Substitution;
参考文献
Wiemann, Arndt; Frank, Ronald; Tegge, Werner
Tetrahedron, 2000 , vol. 56, # 10 p. 1331 - 1337
反应条件
hydrogenchloride in ethyl acetate Yield given;
参考文献
Igano; Minotani; Yoshida; et al.
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3088 - 3094
反应条件
Aliquatreg; 336; sodium hydrogencarbonate in dichloromethane
参考文献
Bocchi,V. et al.
Synthesis, 1979 , p. 957 - 961
反应条件
1: 72 h / 25 °C 2: 1M HCl aq. / ethyl acetate View Scheme
参考文献
Igano; Minotani; Yoshida; et al.
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3088 - 3094
反应条件
1: 72 h / 25 °C 2: 1M HCl aq. / ethyl acetate View Scheme
参考文献
Igano; Minotani; Yoshida; et al.
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3088 - 3094