Cbz-L-天冬氨酸-Alpha苄脂合成路线 (共 22 条)
反应条件
T=90 - 105°C; Yield given;
参考文献
Walczyna, Rita; Sokolowski, Janusz
Carbohydrate Research, 1988 , vol. 180, p. 147 - 151
反应条件
water; sodium hydrogencarbonate anschliessend Behandeln mit Chlorokohlensaeure-benzylester;
参考文献
Bryant et al.
Journal of the Chemical Society, 1959 , p. 3868,3870
反应条件
nitrosyl-sulphuric acid
参考文献
Nefkens,G.H.L.; Nivard,R.J.F.
Recueil des Travaux Chimiques des Pays-Bas, 1965 , vol. 84, p. 1315 - 1318
参考文献
Micheel,F. et al.
Tetrahedron Letters, 1963 , # 2 p. 115 - 119
参考文献
Hayakawa; Harada; Fox
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, # 2 p. 391 - 395
参考文献
Burtin, Guillaume; Corringer, Pierre-Jean; Hitchcock, Peter B.; Young, Douglas W.
Tetrahedron Letters, 1999 , vol. 40, # 22 p. 4275 - 4278
反应条件
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / -15 °C / Inert atmosphere 2: sodium tetrahydroborate / water / 0.17 h / -15 °C / Inert atmosphere 3: Dess-Martin periodane / dichloromethane / 1 h / 20 °C View Scheme
参考文献
Bandyopadhyay, Anupam; Gopi, Hosahudya N.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8089 - 8095
反应条件
1: (i) diethyl-prop-1-ynyl-amine, THF, (ii) aq. NaOH, dioxane 2: CF3CO2H View Scheme
参考文献
Weygand,F. et al.
Chemische Berichte, 1968 , vol. 101, p. 3642 - 3648
反应条件
dicyclohexyl-carbodiimide in dichloromethane
T=0°C; 0.5 h;
参考文献
Matsuo, Ichiro; Isomura, Megumi; Ajisaka, Katsumi
Journal of Carbohydrate Chemistry, 1999 , vol. 18, # 7 p. 841 - 850
参考文献
Bryant et al.
Journal of the Chemical Society, 1959 , p. 3868,3870