Kasymzhanova, M.; Abdukakharov, V. S.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1992 , vol. 28, # 5 p. 525 - 526
Khimiya Prirodnykh Soedinenii, 1992 , # 5 p. 598 - 599
in tetrahydrofuran a suspn. of Rh complex in THF and MeCHCHCH2Br in 1:2 molar ratio sealedin vacuo in a Pyrex reaction tube was either stirred or shaken for 1 h at 20°C; volatiles were removed under vac., trapped at -196°C and analyzed by GLC, residue was chromd. using hexane followed by benzene or CHCl3 as eluent, and recrystd. from a mixt. of either CHCl3 and EtOH or benzene and MeOH;
参考文献
Booth, Brian L.; Casey, Geoffrey C.; Haszeldine, Robert N.
Journal of Organometallic Chemistry, 1982 , vol. 224, # 2 p. 197 - 205
