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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
淡黄霉素
合成路线
（共 17 条）
18512-30-6
萘-1,3,6,8-四酚
→
反应条件
479-05-0
淡黄霉素
反应条件
oxygen; potassium carbonate in N,N-dimethyl-formamide T=25°C; 10 h;
参考文献
Snyder, Scott A.; Tang, Zhen-Yu; Gupta, Ritu
Journal of the American Chemical Society, 2009 , vol. 131, p. 5744 - 5745
2150-44-9
3,5-二羟基苯甲酸甲酯
→
反应条件
479-05-0
淡黄霉素
反应条件
1: 96 percent / K2CO3 / acetone 2: 98 percent / LiAlH4 / diethyl ether 3: 84 percent / NEt3 / CH2Cl2 4: 69 percent / BzNEt3Cl / CHCl3; H2O 5: 92 percent / Ba(OH)2 / dioxane; H2O 6: diethyl ether 7: 99 percent / 60percent HClO4 / H2O; acetic acid 8: 97 percent / H2 / Pd/C (5percent) / ethyl acetate; ethanol 9: CH3ONa / methanol 10: NaBH4 / methanol View Scheme
参考文献
Ichinose, Koji; Ebizuka, Yutaka; Sankawa, Ushio
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2873 - 2875
58605-10-0
3,5-二苄氧基苯甲酸甲酯
→
反应条件
479-05-0
淡黄霉素
反应条件
1: 98 percent / LiAlH4 / diethyl ether 2: 84 percent / NEt3 / CH2Cl2 3: 69 percent / BzNEt3Cl / CHCl3; H2O 4: 92 percent / Ba(OH)2 / dioxane; H2O 5: diethyl ether 6: 99 percent / 60percent HClO4 / H2O; acetic acid 7: 97 percent / H2 / Pd/C (5percent) / ethyl acetate; ethanol 8: CH3ONa / methanol 9: NaBH4 / methanol View Scheme
参考文献
Ichinose, Koji; Ebizuka, Yutaka; Sankawa, Ushio
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2873 - 2875
24131-31-5
3,5-二苄氧基苯甲醇
→
反应条件
479-05-0
淡黄霉素
反应条件
1: 84 percent / NEt3 / CH2Cl2 2: 69 percent / BzNEt3Cl / CHCl3; H2O 3: 92 percent / Ba(OH)2 / dioxane; H2O 4: diethyl ether 5: 99 percent / 60percent HClO4 / H2O; acetic acid 6: 97 percent / H2 / Pd/C (5percent) / ethyl acetate; ethanol 7: CH3ONa / methanol 8: NaBH4 / methanol View Scheme
参考文献
Ichinose, Koji; Ebizuka, Yutaka; Sankawa, Ushio
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2873 - 2875
2732-96-9
3,5-二苄氧基苯甲酸甲酯
→
反应条件
479-05-0
淡黄霉素
反应条件
1: diethyl ether 2: 99 percent / 60percent HClO4 / H2O; acetic acid 3: 97 percent / H2 / Pd/C (5percent) / ethyl acetate; ethanol 4: CH3ONa / methanol 5: NaBH4 / methanol View Scheme
参考文献
Ichinose, Koji; Ebizuka, Yutaka; Sankawa, Ushio
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2873 - 2875
58604-84-5
→
反应条件
479-05-0
淡黄霉素
反应条件
1: 92 percent / Ba(OH)2 / dioxane; H2O 2: diethyl ether 3: 99 percent / 60percent HClO4 / H2O; acetic acid 4: 97 percent / H2 / Pd/C (5percent) / ethyl acetate; ethanol 5: CH3ONa / methanol 6: NaBH4 / methanol View Scheme
参考文献
Ichinose, Koji; Ebizuka, Yutaka; Sankawa, Ushio
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2873 - 2875
79762-35-9
→
反应条件
479-05-0
淡黄霉素
反应条件
1: 99 percent / 60percent HClO4 / H2O; acetic acid 2: 97 percent / H2 / Pd/C (5percent) / ethyl acetate; ethanol 3: CH3ONa / methanol 4: NaBH4 / methanol View Scheme
参考文献
Ichinose, Koji; Ebizuka, Yutaka; Sankawa, Ushio
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2873 - 2875
65857-78-5
→
反应条件
479-05-0
淡黄霉素
反应条件
1: 97 percent / H2 / Pd/C (5percent) / ethyl acetate; ethanol 2: CH3ONa / methanol 3: NaBH4 / methanol View Scheme
参考文献
Ichinose, Koji; Ebizuka, Yutaka; Sankawa, Ushio
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2873 - 2875
80457-61-0
→
反应条件
479-05-0
淡黄霉素
反应条件
1: 69 percent / BzNEt3Cl / CHCl3; H2O 2: 92 percent / Ba(OH)2 / dioxane; H2O 3: diethyl ether 4: 99 percent / 60percent HClO4 / H2O; acetic acid 5: 97 percent / H2 / Pd/C (5percent) / ethyl acetate; ethanol 6: CH3ONa / methanol 7: NaBH4 / methanol View Scheme
参考文献
Ichinose, Koji; Ebizuka, Yutaka; Sankawa, Ushio
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2873 - 2875
71741-18-9
→
反应条件
479-05-0
淡黄霉素
反应条件
1: With palladium on activated charcoal; sodium acetate; acetic anhydride 2: With potassium carbonate in ethanol
参考文献
Vagstad, Anna L.; Hill, Eric A.; Labonte, Jason W.; Townsend, Craig A.
Chemistry and Biology, 2012 , vol. 19, # 12 p. 1525 - 1534
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