6H-苯并呋喃并[3,2-c][1]苯并吡喃-6-酮合成路线 （共 54 条）
反应条件
1: 90 percent / aq. NaOH / methanol / 0.5 h / 20 °C
2: 35 percent / CuCl2; NaOAc; K2CO3 / PdCl2 / acetonitrile / 20 h / 20 °C
View Scheme
参考文献
Hiroya, Kou; Suzuki, Naoyuki; Yasuhara, Akito; Egawa, Yuya; Kasano, Atsushi; Sakamoto, Takao
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 24 p. 4339 - 4346
反应条件
2: 90 percent / PhMe3Si, I2 / 3 h / 110 °C
View Scheme
参考文献
Larock, Richard C.; Harrison, L. Wayne
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4218 - 4227
反应条件
1: 96 percent / 12 M aq. HCl / CHCl3 / 24 h / 20 °C
2: 68 percent / air / 10percent Pd on C / diphenyl ether / 48 h / 240 °C
View Scheme
参考文献
Maischein, Juergen; Vilsmaier, Elmar
Liebigs Annalen der Chemie, 1988 , p. 355 - 370
反应条件
1: 59 percent / toluene / 0.5 h / Heating
2: 96 percent / 12 M aq. HCl / CHCl3 / 24 h / 20 °C
3: 68 percent / air / 10percent Pd on C / diphenyl ether / 48 h / 240 °C
View Scheme
参考文献
Maischein, Juergen; Vilsmaier, Elmar
Liebigs Annalen der Chemie, 1988 , p. 355 - 370
反应条件
Pd(dba-4-OMe)2; caesium carbonate; triphenylphosphine in tetrahydrofuran
T=70°C; Inert atmosphere;
参考文献
Burns, Michael J.; Thatcher, Robert J.; Taylor, Richard J. K.; Fairlamb, Ian J. S.
Dalton Transactions, 2010 , vol. 39, # 43 p. 10391 - 10400
反应条件
1: 95 percent / I2 / CH2Cl2 / 12 h / 25 °C
2: 99 percent / PdCl2(PPh3)2; K2CO3 / dimethylformamide / 6 h / 60 °C
View Scheme
参考文献
Yao, Tuanli; Yue, Dawei; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 9985 - 9989
反应条件
1: 96 percent / CuI; PdCl2(PPh3)2; Et3N / dimethylformamide / 2 h / 60 °C
2: 95 percent / I2 / CH2Cl2 / 12 h / 25 °C
3: 99 percent / PdCl2(PPh3)2; K2CO3 / dimethylformamide / 6 h / 60 °C
View Scheme
参考文献
Yao, Tuanli; Yue, Dawei; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 9985 - 9989
反应条件
1: benzene / 48 h / 20 °C / Irradiation
2: aq. HCl / tetrahydrofuran / 36 h / 50 °C
View Scheme
参考文献
Kraus, George A.; Zhang, Ning
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5644 - 5646
反应条件
in hexane
Irradiation;
参考文献
Chiang, Yvonne; Gaplovsky, Martin; Kresge, A. Jerry; Leung, King Hung; Ley, Christian; Mac, Marek; Persy, Gabriele; Phillips, David L.; Popik, Vladimir V.; Roedig, Christoph; Wirz, Jakob; Zhu, Yu
Journal of the American Chemical Society, 2003 , vol. 125, # 42 p. 12872 - 12880
反应条件
1: 61 percent
2: pyridine hydrochloride / Heating
3: 60 percent / DDQ / benzene / Heating
View Scheme
参考文献
Mali, R. S.; Tilve, S. G.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 465
