5,6-二羟基-2-吲哚甲酸合成路线 (共 23 条)
反应条件
1: water; sodium hydroxide / ethanol / 20 °C 2: boron tribromide / dichloromethane / -78 - 20 °C View Scheme
参考文献
ACS Medicinal Chemistry Letters, , vol. 3, # 7 p. 550 - 554
反应条件
1: sodium methoxide / methanol / 4 h / -15 °C 2: xylene / 0.25 h / Heating 3: KOH / H2O / 1 h / Heating 4: BBr3; H2O / CH2Cl2 / 4 h / -40 °C View Scheme
参考文献
Molecules, , vol. 11, # 12 p. 968 - 977
反应条件
1: sodium methoxide / methanol / 4 h / -15 °C 2: xylene / 0.25 h / Heating 3: KOH / H2O / 1 h / Heating 4: BBr3; H2O / CH2Cl2 / 4 h / -40 °C View Scheme
参考文献
Molecules, , vol. 11, # 12 p. 968 - 977
反应条件
1: KOH / H2O / 1 h / Heating 2: BBr3; H2O / CH2Cl2 / 4 h / -40 °C View Scheme
参考文献
Molecules, , vol. 11, # 12 p. 968 - 977
反应条件
1: xylene / 0.25 h / Heating 2: KOH / H2O / 1 h / Heating 3: BBr3; H2O / CH2Cl2 / 4 h / -40 °C View Scheme
参考文献
Molecules, , vol. 11, # 12 p. 968 - 977
反应条件
1: KOH / H2O / 1 h / Heating 2: BBr3; H2O / CH2Cl2 / 4 h / -40 °C View Scheme
参考文献
Molecules, , vol. 11, # 12 p. 968 - 977
反应条件
1: xylene / 0.25 h / Heating 2: KOH / H2O / 1 h / Heating 3: BBr3; H2O / CH2Cl2 / 4 h / -40 °C View Scheme
参考文献
Molecules, , vol. 11, # 12 p. 968 - 977
反应条件
methanol; sodium hydroxide; sodium dithionite T=0°C;
参考文献
Journal of the Chemical Society, , p. 2061,2064
反应条件
dihydrogen peroxide; potassium carbonate T=25°C; diferent time; Product distribution;
参考文献
Tetrahedron, , vol. 51, # 20 p. 5913 - 5920
反应条件
zinc diacetate in various solvent(s) Ambient temperaturerearrengament time; MechanismProduct distribution;
参考文献
Gazzetta Chimica Italiana, , vol. 115, # 7 p. 357 - 360