3-苯基-1,4-环己二烯合成路线 (共 9 条)
反应条件
ammonia; lithium in diethyl ether; water
T=-78 - -25°C; 0.5 h;
参考文献
Durie, Alastair J.; Fujiwara, Tomoya; Cormanich, Rodrigo; Buehl, Michael; Slawin, Alexandra M. Z.; O'Hagan, David
Chemistry - A European Journal, 2014 , vol. 20, # 21 p. 6259 - 6263
反应条件
diisopropylamine in acetonitrile
5 h; Irradiation;
参考文献
Tanaka, Yoshio; Tsujimoto, Kazuo; Ohashi, Mamoru
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 788 - 790
反应条件
in methanol
Irradiation;
参考文献
Williams,J.L.R. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 53 - 55
反应条件
1: With ammonia; calcium in tetrahydrofuran
T=-60°C; Birch Reduction; 0.5 h; Inert atmosphereSchlenk technique;
2: With methanol in tetrahydrofuran
Birch Reduction; Inert atmosphereSchlenk technique; Overall yield = 82 percent; Overall yield = 2.49 g;
参考文献
Koehler, Mathias; Langer, Jens; Fischer, Reinald; Goerls, Helmar; Westerhausen, Matthias
Chemistry - A European Journal, 2013 , vol. 19, # 32 p. 10497 - 10500
反应条件
ethanol; calcium
T=20°C; 24 h;
参考文献
Mitoma; Nagashima; Simion; Yamada; Mimura; Ishimoto; Tashiro
Environmental Science and Technology, 2001 , vol. 35, # 20 p. 4145 - 4148
反应条件
in acetonitrile
5 h; Irradiation;
参考文献
Tanaka, Yoshio; Tsujimoto, Kazuo; Ohashi, Mamoru
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 788 - 790
参考文献
De Tar; Long
Journal of the American Chemical Society, 1958 , vol. 80, p. 4742
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Lynch; Pausacker
Australian Journal of Chemistry, 1957 , vol. 10, p. 40,42
参考文献
Hey,D.H. et al.
Journal of the Chemical Society, 1963 , p. 5604 - 5611
Full Text Show Details
De Tar; Long
Journal of the American Chemical Society, 1958 , vol. 80, p. 4742
反应条件
P=5 - 30 Torr; Irradiationproduct yields as function of laser energies (20-550 mJ/cm2); Product distribution;
参考文献
Kauer, M.; Wagner, H. Gg.
Zeitschrift fuer Physikalische Chemie (Muenchen, Germany), 1987 , vol. 153, p. 109 - 128