N-Boc-4-甲氧基亚苄基胺合成路线 （共 4 条）
反应条件
potassium carbonate; sodium sulfate in tetrahydrofuran
15 h; RefluxInert atmosphere;
参考文献
Seayad, Abdul Majeed; Ramalingam, Balamurugan; Yoshinaga, Kazuhiko; Nagata, Takushi; Chai, Christina L. L.
Organic Letters, 2010 , vol. 12, # 2 p. 264 - 267
反应条件
1: formic acid / methanol; H2O / 72 h / 20 °C
2: anhydrous potassium carbonate / tetrahydrofuran / 17 h / Heating
View Scheme
参考文献
Palomo, Claudio; Oiarbide, Mikel; Halder, Rajkumar; Laso, Antonio; Lopez, Rosa
Angewandte Chemie - International Edition, 2006 , vol. 45, # 1 p. 117 - 120
反应条件
potassium hydride in dichloromethane
T=20°C; 1 h;
参考文献
Enders, Dieter; Oberboersch, Stefan
Synlett, 2002 , # 3 p. 471 - 473
反应条件
1: formic acid / methanol; H2O / 72 h / 20 °C
2: anhydrous potassium carbonate / tetrahydrofuran / 17 h / Heating
View Scheme
参考文献
Palomo, Claudio; Oiarbide, Mikel; Halder, Rajkumar; Laso, Antonio; Lopez, Rosa
Angewandte Chemie - International Edition, 2006 , vol. 45, # 1 p. 117 - 120
