2,2'-联噻吩-5-硼酸频哪醇酯合成路线 (共 15 条)
反应条件
sodium carbonate; bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether; ethanol Suzuki reaction; 48 h; Heating;
参考文献
Bandini, Marco; Melucci, Manuela; Piccinelli, Fabio; Sinisi, Riccardo; Tommasi, Simona; Umani-Ronchi, Achille
Chemical Communications, 2007 , # 43 p. 4519 - 4521
反应条件
aluminum oxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride T=90°C; Suzuki coupling; 0.166667 h; microwave irradiation;
参考文献
Melucci, Manuela; Barbarella, Giovanna; Sotgiu, Giovanna
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 8877 - 8884
反应条件
potassium fluoride in water; N,N-dimethyl-formamide T=140°C; 0.0833333 h; Microwave irradiation;
参考文献
Dimaria, Francesca; Barbarella, Giovanna
Journal of Sulfur Chemistry, 2013 , vol. 34, # 6 p. 627 - 637
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; water; toluene T=95°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Hassan Omar, Omar; Babudri, Francesco; Farinola, Gianluca M.; Naso, Francesco; Operamolla, Alessandra; Pedone, Adriana
Tetrahedron, 2011 , vol. 67, # 2 p. 486 - 494
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethanol; toluene T=75°C; Suzuki coupling reaction; 0.75 h;
参考文献
Leroy, Julie; Boucher, Nicolas; Sergeyev, Sergey; Sferrazza, Michele; Geerts, Yves Henri
European Journal of Organic Chemistry, 2007 , # 8 p. 1256 - 1261