2-(alpha-甲基苄基氧基)-乙醇合成路线 (共 12 条)
反应条件
anhydrous iron chloride; toluene-4-sulfonic acid in chlorobenzene
T=80°C; 24 h;
参考文献
Ke, Fang; Li, Zhengkai; Xiang, Haifeng; Zhou, Xiangge
Tetrahedron Letters, 2011 , vol. 52, # 2 p. 318 - 320
反应条件
sodium tetrahydroborate; zirconium tetrachloride in tetrahydrofuran
6 h; Ambient temperature;
参考文献
Purushothama Chary; Santosh Laxmi; Iyengar
Synthetic Communications, 1999 , vol. 29, # 8 p. 1257 - 1261
反应条件
boron trifluoride diethyl etherate; (-)-sparteine in diethyl ether
T=-78°C;
参考文献
Mueller, Paul; Nury, Patrice; Bernardinelli, Gerald
European Journal of Organic Chemistry, 2001 , # 21 p. 4137 - 4147
参考文献
Miyake, Hideyoshi; Fujimura, Masahiro; Tsumura, Takatsugu; Sasaki, Mitsuru
Chemistry Letters, 2006 , vol. 35, # 7 p. 778 - 779
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether
T=30°C; Reduction; 12 h;
参考文献
Shaozu, Wu; Tianhui, Ren; Ning, Chen; Yulan, Zhang
Organic Preparations and Procedures International, 1991 , vol. 23, # 4 p. 427 - 431
反应条件
sodium cyanide
T=140 - 150°C;
参考文献
Dow Chem. Co.
Patent: US2620359 , 1947 ;
反应条件
potassium hydroxide; dibenzo-18-crown-6
T=80°C;
参考文献
Petrov; Ozerov; Novikov; Pannecouque; Balzarini; De Clercq
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 9 p. 1218 - 1226
参考文献
Miyake, Hideyoshi; Fujimura, Masahiro; Tsumura, Takatsugu; Sasaki, Mitsuru
Chemistry Letters, 2006 , vol. 35, # 7 p. 778 - 779
反应条件
lithium aluminium tetrahydride; (η5-C5H5)titanium trichloride in diethyl ether
12 h; Heating; Title compound not separated from byproducts;
参考文献
Shaozu, Wu; Yin, Chen; Yulan, Zhang
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 5 p. 421 - 424
反应条件
AuCl3-CuCl2
5.7 h; Heating;
参考文献
Zhang, Xin; Corma, Avelino
Chemical Communications, 2007 , # 29 p. 3080 - 3082