3-苄氧基-1,2-丙二醇合成路线 （共 49 条）
反应条件
antimony trichloride in water; acetonitrile T=20°C; 0.166667 h;
参考文献
Wu, Qinpei; Wang, Yuan; Chen, Wei; Liu, Hua
Synthetic Communications, 2006 , vol. 36, # 10 p. 1361 - 1366
反应条件
1: With potassium hydroxide in benzene Etherification; 23 h; Heating; 2: With toluene-4-sulfonic acid in methanol; dichloromethane T=20°C; Ring cleavage; 5 h;
参考文献
Bhattacharya, Santanu; Dileep
Tetrahedron Letters, 1999 , vol. 40, # 46 p. 8167 - 8171
反应条件
hydrogenchloride in ethanol; chloroform; ethyl acetate; acetone
参考文献
G. D. Searle and Co.
Patent: US4567189 A1, 1986 ;
反应条件
sodium hydroxide; sulfuric acid in water
参考文献
Senju Pharmaceutical Co., Ltd.
Patent: US5098898 A1, 1992 ;
反应条件
ammonium cerium(IV) nitrate; water in acetonitrile T=20°C; 2 h;
参考文献
Jana; Roy
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2007 , vol. 46, # 4 p. 707 - 709
反应条件
RuHCl(CO)(bis-(2-diphenylphosphinoethyl)amine); potassium tert-butylate; hydrogen in tetrahydrofuran T=140°C; 4 h; Autoclave;
参考文献
Han, Zhaobin; Rong, Liangce; Wu, Jiang; Zhang, Lei; Wang, Zheng; Ding, Kuiling
Angewandte Chemie - International Edition, 2012 , vol. 51, # 52 p. 13041 - 13045
Angew. Chem., 2012 , vol. 124, # 52
反应条件
sodium phosphate buffer in di-isopropyl ether T=10°C; 24 h; Yields of byproduct given;
参考文献
Matsumoto, Kazutsugu; Fuwa, Seiji; Kitajima, Hidehiko
Tetrahedron Letters, 1995 , vol. 36, # 36 p. 6499 - 6502
反应条件
1: NaH 2: H2O / acetic acid View Scheme
参考文献
Shiao, Min-Jen; Yang, Chia-Yu; Lee, Shi-Hung; Wu, Teh-Chun
Synthetic Communications, 1988 , vol. 18, # 4 p. 359 - 366
反应条件
lithium amide; ammonia in tetrahydrofuran 0.166667 h;
参考文献
Chandrasekhar; Srinivas, Ch.; Srihari
Synthetic Communications, 2003 , vol. 33, # 6 p. 895 - 902
反应条件
sodium tetrahydroborate in ethanol; dichloromethane T=0°C; Reduction; 0.333333 h;
参考文献
Marguet, Frank; Cavalier, Jean-Francois; Verger, Robert; Buono, Gerard
European Journal of Organic Chemistry, 1999 , # 7 p. 1671 - 1678
