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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
紫云英苷
合成路线
（共 32 条）
256442-36-1
→
反应条件
480-10-4
紫云英苷
+
22153-44-2
5,7-二羟基-2-(4-羟基苯基)-4-氧代-4H-苯并吡喃-3-基6-O-[(2Z)-3-(4-羟基苯基)-2-丙烯酰基]-beta-D-吡喃葡萄糖苷
反应条件
sodium methylate in methanol; chloroform 2 h; Ambient temperature;
参考文献
Vermes, Barbara; Chari, Vedanta Mohan; Wagner, Hildebert
Helvetica Chimica Acta, 1981 , vol. 64, # 6 p. 1964 - 1968
877621-21-1
→
反应条件
480-10-4
紫云英苷
反应条件
sodium methylate in methanol T=20°C; pH=8; 2 h;
参考文献
Zhu, Yujin; Zhang, Yanjun; Liu, Yi; Chu, Hongwan; Duan, Hongquan
Molecules, 2010 , vol. 15, # 12 p. 9174 - 9183
133-89-1
尿苷(5')二氢二磷酰(1)-alpha-D-葡萄糖
+
520-18-3
山奈酚
→
反应条件
480-10-4
紫云英苷
反应条件
UDP glucose:flavonol glucosyltransferase enzyme preparation from Norway spruce needles in water 0.75 h; pH 8.0 bicine buffer;
参考文献
Ren, Guangxiang; Hou, Jingli; Fang, Qinghong; Sun, Hong; Liu, Xiaoyan; Zhang, Lianwen; Wang, Peng George
Glycoconjugate Journal, 2012 , vol. 29, # 5-6 p. 425 - 432
152390-63-1
→
反应条件
480-10-4
紫云英苷
反应条件
sodium acetate in water T=37°C; 336 h; cellulase;
参考文献
Sekine; Arai; Ikegami; Fujii; Shindo; Yanagisawa; Ishida; Okonogi; Murakoshi
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 6 p. 1185 - 1187
56317-05-6
→
反应条件
480-10-4
紫云英苷
反应条件
sodium carbonate in methanol; dimethyl sulfoxide T=40°C;
参考文献
Masuda; Iritani; Yonemori; Oyama; Takeda
Bioscience, biotechnology, and biochemistry, 2001 , vol. 65, # 6 p. 1302 - 1309
76343-90-3
→
反应条件
480-10-4
紫云英苷
反应条件
ammonium hydroxide in methanol 48 h; Ambient temperature;
参考文献
Isobe,T.; Ito,N.
Phytochemistry (Elsevier), 1980 , vol. 19, p. 1877
23405-70-1
→
反应条件
480-10-4
紫云英苷
反应条件
1: acetic acid / water / 110 °C 2: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C 3: methanol; sodium methylate / 5 h / 20 °C 4: hydrogen; palladium(II) oxide hydrate / tetrahydrofuran; methanol / 6 h / 20 °C View Scheme
参考文献
Yamasaki, Kazuaki; Hishiki, Ryogo; Kato, Eisuke; Kawabata, Jun
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 1 p. 17 - 21
96333-59-4
→
反应条件
480-10-4
紫云英苷
反应条件
1: 3,3-dimethyldioxirane / dichloromethane; acetone / 0 °C 2: acetic acid / water / 110 °C 3: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C 4: methanol; sodium methylate / 5 h / 20 °C 5: hydrogen; palladium(II) oxide hydrate / tetrahydrofuran; methanol / 6 h / 20 °C View Scheme
参考文献
Yamasaki, Kazuaki; Hishiki, Ryogo; Kato, Eisuke; Kawabata, Jun
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 1 p. 17 - 21
30652-27-8
→
反应条件
480-10-4
紫云英苷
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C 2: methanol; sodium methylate / 5 h / 20 °C 3: hydrogen; palladium(II) oxide hydrate / tetrahydrofuran; methanol / 6 h / 20 °C View Scheme
参考文献
Yamasaki, Kazuaki; Hishiki, Ryogo; Kato, Eisuke; Kawabata, Jun
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 1 p. 17 - 21
480-66-0
2,4,6-三羟基苯乙酮一水合物
→
反应条件
480-10-4
紫云英苷
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 20 °C 2: sodium hydride / N,N-dimethyl-formamide / 20 °C 3: iodine / dimethyl sulfoxide / 110 °C 4: 3,3-dimethyldioxirane / dichloromethane; acetone / 0 °C 5: acetic acid / water / 110 °C 6: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C 7: methanol; sodium methylate / 5 h / 20 °C 8: hydrogen; palladium(II) oxide hydrate / tetrahydrofuran; methanol / 6 h / 20 °C View Scheme
参考文献
Yamasaki, Kazuaki; Hishiki, Ryogo; Kato, Eisuke; Kawabata, Jun
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 1 p. 17 - 21
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