2,4,6-三甲基苯甲酸合成路线 (共 191 条)
反应条件
1: diphenyl diselenide With AlCl3, aluminium chloride; zinc in acetonitrile T=70°C; P=760.051 Torr; 1.25 h; Neutral; 2: methyl 2,4,6-trimethylbenzoate in acetonitrile T=70°C; P=760.051 Torr; 6 h; Neutral;
参考文献
Nazari, Mohammad; Movassagh, Barahman
Tetrahedron Letters, 2009 , vol. 50, # 4 p. 438 - 441
反应条件
Li(1+)*C12H28AlO3(1-) in tetrahydrofuran; hexane T=-78°C; 1 h;
参考文献
Kim, Sunggak; Ahn, Kyo Han
Journal of Organic Chemistry, 1984 , vol. 49, # 10 p. 1717 - 1724
反应条件
Me2AlTeMe in toluene T=23°C; 12 h;
参考文献
Reddy, B.V. Subba; Reddy, Leleti Rajender; Corey
Tetrahedron Letters, 2005 , vol. 46, # 27 p. 4589 - 4593
反应条件
Me2AlTeMe in toluene T=23°C; 14 h;
参考文献
Reddy, B.V. Subba; Reddy, Leleti Rajender; Corey
Tetrahedron Letters, 2005 , vol. 46, # 27 p. 4589 - 4593
反应条件
palladium diacetate in acetic acid 7 h; Heating; Yield given;
参考文献
Grushin, Vladimir V.; Marshall, William J.; Thorn, David L.
Advanced Synthesis and Catalysis, 2001 , vol. 343, # 2 p. 161 - 165
反应条件
sodium hydroxide; Aliquatreg; 336 T=200°C; 0.0833333 h; microwave irradiation;
参考文献
Perreux, Laurence; Loupy, Andre
Organic Preparations and Procedures International, 2003 , vol. 35, # 4 p. 361 - 368
反应条件
aluminum tri-bromide P=44130.5 Torr;
参考文献
Norris; Wood
Journal of the American Chemical Society, 1940 , vol. 62, p. 1428,1431
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; sodium hydroxide in tetrahydrofuran 48 h; Ambient temperature; Further byproducts given;
参考文献
Ashby, E. C.; Coleman, David; Gamasa, Maria
Journal of Organic Chemistry, 1987 , vol. 52, # 18 p. 4079 - 4085
反应条件
potassium permanganate; acetone; magnesium chloride
参考文献
Bailey; Burr
Journal of the American Chemical Society, 1953 , vol. 75, p. 2951,2954
反应条件
potassium hydroxide in tert-butyl alcohol T=50°C; Electrochemical reaction; Title compound not separated from byproducts.;
参考文献
Lyalin; Petrosyan
Russian Chemical Bulletin, 2007 , vol. 56, # 3 p. 499 - 503