2,4,6-三甲基苯甲酸合成路线 （共 191 条）
反应条件
[Ru(η5-C5H5)(PPh3)(NCCH3)2][PF6]; diethylene glycol dimethyl ether; water in tetrahydrofuran; dichloromethane T=85°C; 1 h; Inert atmosphere;
参考文献
Nakamura, Asami; Hamasaki, Akiyuki; Goto, Sachihiko; Utsunomiya, Masaru; Tokunaga, Makoto
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 6 p. 973 - 984
反应条件
T=200°C; 0.166667 h;
参考文献
Oida, Tatsuo; Shimizu, Tomio; Hayashi, Yoshiyuki; Teramura, Kazuhiro
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 5 p. 1429 - 1433
反应条件
bei der Destillation;
参考文献
van Scherpenzeel
Recueil des Travaux Chimiques des Pays-Bas, 1900 , vol. 19, p. 377
反应条件
1: magnesium / tetrahydrofuran / 0.33 h / 80 °C / microwave irradiation 2: 74 percent / tetrahydrofuran / 0.08 h / 1 °C View Scheme
参考文献
Khaibulova, T. Sh.; Boyarskaya; Boyarskii
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 3 p. 360 - 365
Zh. Org. Khim., 2013 , vol. 49, # 3 p. 373 - 378
反应条件
1: 81 percent / triethylamine / benzene / 48 h 2: 30 percent / 0.17 h / 200 °C View Scheme
参考文献
Oida, Tatsuo; Shimizu, Tomio; Hayashi, Yoshiyuki; Teramura, Kazuhiro
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 5 p. 1429 - 1433
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione T=70°C; 2 h;
参考文献
Moorthy, Jarugu Narasimha; Singhal, Nidhi; Venkatakrishnan
Tetrahedron Letters, 2004 , vol. 45, # 28 p. 5419 - 5424
反应条件
nitric acid T=115 - 130°C; im geschlossenen Rohr;
参考文献
Jacobsen
Chemische Berichte, 1882 , vol. 15, p. 1854
Full Text Show Details
Jannasch; Weiler
Chemische Berichte, 1894 , vol. 27, p. 3444
Chemische Berichte, 1895 , vol. 28, p. 531
反应条件
nitric acid T=115 - 130°C; im geschlossenen Rohr;
参考文献
Jannasch; Weiler
Chemische Berichte, 1895 , vol. 28, p. 531
反应条件
T=200°C; 0.166667 h;
参考文献
Oida, Tatsuo; Shimizu, Tomio; Hayashi, Yoshiyuki; Teramura, Kazuhiro
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 5 p. 1429 - 1433
反应条件
T=20°C; P=44130.5 Torr;
参考文献
Norris; Wood
Journal of the American Chemical Society, 1940 , vol. 62, p. 1428,1431
