2,4,6-三羟基苯乙酮一水合物合成路线 （共 215 条）
反应条件
monoacetylphloroglucinol acetyltransferase T=25°C; pH=7; aq. phosphate bufferEnzymatic reaction; Kinetics;
参考文献
Hayashi, Asuka; Saitou, Hiroki; Mori, Tomomi; Matano, Ikue; Sugisaki, Hiroyuki; Maruyama, Kiyofumi
Bioscience, Biotechnology and Biochemistry, 2012 , vol. 76, # 3 p. 559 - 566
反应条件
in Aether und Erhitzen des Reaktionsprodukts mit Wasser;
参考文献
Gruber; Traub
Monatshefte fuer Chemie, 1947 , vol. 77, p. 414,423
反应条件
1: potassium carbonate / acetone / 0 - 20 °C 2: potassium hydroxide / ethanol 3: sodium acetate / ethanol / Reflux 4: hydrogenchloride / methanol; water / 0.5 h / Reflux View Scheme
参考文献
Zhao, Dong-Hai; Sui, Xin; Qu, You-Le; Yang, Li-Ye; Wang, Xian; Guan, Li-Ping
Asian Journal of Chemistry, 2011 , vol. 23, # 3 p. 1129 - 1132
反应条件
1: potassium carbonate / acetone
2: potassium hydroxide / methanol / 12 h / 50 °C / |Inert atmosphere
View Scheme
参考文献
Seo, Young Ho; Park, Sun You
Bulletin of the Korean Chemical Society, 2014 , vol. 35, # 4 p. 1154 - 1158
反应条件
sodium hydride in N,N-dimethyl-formamide
2 h; Ambient temperature;
参考文献
Yang, Lei Xiang; Huang, Ke Xin; Li, Hai Bo; Gong, Jing Xu; Wang, Feng; Feng, Yu Bing; Tao, Qiao Feng; Wu, Yi Hang; Li, Xiao Kun; Wu, Xiu Mei; Zeng, Su; Spencer, Shawn; Zhao, Yu; Qu, Jia
Journal of Medicinal Chemistry, 2009 , vol. 52, # 23 p. 7732 - 7752
反应条件
1: 73 percent / N,N-diisopropylethylamine / tetrahydrofuran / 12 h / 0 °C
2: 1.) NaH (80percent in oil) / 1.) THF, 0 deg C, 30 min; 2.) THF, 0 deg C, 30 min
View Scheme
参考文献
Choi, Yoon-Jung; Shim, Pil-Jong; Ko, Kyung-Soo; Kim, Hee-Doo
Heterocycles, 1996 , vol. 43, # 6 p. 1223 - 1228
反应条件
1.1: K2CO3 / acetone / 0.17 h / 20 °C
1.2: 30 percent / acetone / 24 h / Heating
2.1: ZnCl2; AcOH / 2 h / 140 - 150 °C
3.1: 63 mg / aq. NaOH; aq. H2O2 / 3 h / cooling
4.1: 82 percent / aq. HBr; acetic acid / 23 h / Heating
View Scheme
参考文献
Rao et al.
Proceedings - Indian Academy of Sciences, Section A, 1949 , # 29 p. 72,75
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in dichloromethane; water
T=20°C; 24 h;
参考文献
Vogel, Susanne; Heilmann, Joerg
Journal of Natural Products, 2008 , vol. 71, # 7 p. 1237 - 1241
反应条件
potassium carbonate in acetone
3 h; Heating; Yield given. Yields of byproduct given;
参考文献
Tada, Akihiro; Saitoh, Tamotsu; Shoji, Junzo
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 8 p. 2487 - 2493
反应条件
potassium carbonate; acetone
参考文献
Curd; Robertson
Journal of the Chemical Society, 1933 , p. 437,440
Full Text Show Details
Gruber; Traub
Monatshefte fuer Chemie, 1947 , vol. 77, p. 414,423
