2,4,6-三羟基苯乙酮一水合物合成路线 （共 215 条）
反应条件
1: 92 percent / K2CO3 / acetone / 3 h / 65 °C
2: 60 percent / aluminium chloride / chlorobenzene / 1 h / Heating
3: 99 percent / K2CO3 / acetone / Heating
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参考文献
Srivastava, Savitri D.; Srivastava, Santosh K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 57 - 58
反应条件
1: 10 percent / diphenyl ether / 3 h / Heating
2: 12 percent / aq. NaOH; aq. H2O2 / 3 h / cooling
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参考文献
Gao, Hong; Kawabata, Jun
Bioscience, Biotechnology and Biochemistry, 2004 , vol. 68, # 9 p. 1858 - 1864
反应条件
1: sodium-<3,4,5-trimethoxy benzoate> / 175 °C / anschliessend Erwaermen mit wss.-aethanol. Kalilauge und Erwaermen des Reaktionsprodukts mit Essigsaeure
2: aqueous hydriodic acid; acetic acid anhydride
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参考文献
Anderson
Canadian Journal of Research, 1932 , vol. 7, p. 285,289
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Badhwar; Kang; Venkataraman
Journal of the Chemical Society, 1932 , p. 1107,1108
反应条件
1.1: K2CO3 / acetone / 0.17 h / 20 °C
1.2: 32 percent / acetone / 24 h / Heating
2.1: ZnCl2; AcOH / 2 h / 140 - 150 °C
3.1: 76 mg / aq. NaOH; aq. H2O2 / 3 h / cooling
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参考文献
Gao, Hong; Kawabata, Jun
Bioscience, Biotechnology and Biochemistry, 2004 , vol. 68, # 9 p. 1858 - 1864
反应条件
1: potassium carbonate / acetone
2: potassium hydroxide / ethanol
3: hydrogenchloride / methanol; water / 0.5 h / Reflux
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参考文献
Sui, Xin; Quan, Ying-Chun; Chang, Yue; Zhang, Rui-Peng; Xu, Yin-Feng; Guan, Li-Ping
Medicinal Chemistry Research, 2012 , vol. 21, # 7 p. 1290 - 1296
