烯丙基-α-D-吡喃半乳糖苷合成路线 (共 9 条)
反应条件
Kluyveromyces lactis β-galactosidase T=37°C; 24 h; Enzymatic reaction;
参考文献
Rauter, Marion; Schwarz, Maria; Becker, Karin; Baronian, Keith; Bode, Ruediger; Kunze, Gotthard; Vorbrodt, H.-Matthias
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 97, p. 319 - 327
反应条件
Dowex-50 X-8 1.5 h; Heating;
参考文献
El-Shenawy; Schuerch
Carbohydrate research, 1984 , vol. 131, # 2 p. 227 - 238
反应条件
boron trifluoride diethyl etherate 3 h; Heating;
参考文献
Goebel, Matthias; Nothofer, Heinz-Georg; Ross, Guenther; Ugi, Ivar
Tetrahedron, 1997 , vol. 53, # 9 p. 3123 - 3134
反应条件
trifluoroacetic acid T=105°C; Fischer glycosidation; 26 h;
参考文献
Gorityala, Bala Kishan; Ma, Jimei; Pasunooti, Kalyan Kumar; Cai, Shuting; Liu, Xue-Wei
Green Chemistry, 2011 , vol. 13, # 3 p. 573 - 577
反应条件
gold(III) chloride in acetonitrile T=82°C; 7 h; Inert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Mamidyala, Sreeman K.; Finn
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8417 - 8420
反应条件
jack-bean meal in water T=40°C; 96 h; pH=6.6;
参考文献
Nilsson, Kurt G. I.
Carbohydrate Research, 1988 , vol. 180, p. 53 - 60
反应条件
gold(III) chloride in acetonitrile 4 h; RefluxInert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Mamidyala, Sreeman K.; Finn
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8417 - 8420
反应条件
anhydrous iron chloride T=60 - 70°C; modified Fischer-Lubineau reaction; P=7500.75 Torr; 1.08333 h; Microwave irradiation; optical yield given as percent de;
参考文献
Santra, Soumava; Jonas, Emily; Bourgault, Jean-Paul; El-Baba, Tarick; Andreana, Peter R.
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 1 p. 27 - 40
参考文献
Pacsu; Ticharich
Chemische Berichte, 1929 , vol. 62, p. 3008,3011