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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
异槲皮苷
合成路线
（共 36 条）
53171-28-1
→
反应条件
482-35-9
异槲皮苷
反应条件
sodium carbonate in methanol; dimethyl sulfoxide T=40°C;
参考文献
Masuda; Iritani; Yonemori; Oyama; Takeda
Bioscience, biotechnology, and biochemistry, 2001 , vol. 65, # 6 p. 1302 - 1309
108-93-0
环己醇
→
反应条件
482-35-9
异槲皮苷
反应条件
formic acid; water
参考文献
Fox et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 2504
117-39-5
槲皮素
+
572-09-8
乙酰溴-α-D-葡萄糖
→
反应条件
482-35-9
异槲皮苷
+
20229-56-5
绣线菊甙
反应条件
1: With potassium carbonate in dimethyl sulfoxide Koenigs-Knorr reaction; 2: With sodium methylate in methanol T=20°C; 0.333333 h;
参考文献
Murota, Kaeko; Mitsukuni, Yuki; Ichikawa, Mami; Tsushida, Tojiro; Miyamoto, Sayuri; Terao, Junji
Journal of agricultural and food chemistry, 2004 , vol. 52, # 7 p. 1907 - 1912
83144-69-8
→
反应条件
482-35-9
异槲皮苷
反应条件
hydrogenchloride in methanol 0.0166667 h; Heating;
参考文献
Romussi; Lucchesini
Pharmazie, 1993 , vol. 48, # 3 p. 227 - 228
13459-13-7
→
反应条件
482-35-9
异槲皮苷
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 32 h / 20 °C / Inert atmosphere 2: sodium methylate / methanol / 9.5 h / 20 °C / Inert atmosphere 3: palladium 10 on activated carbon; hydrogen / ethanol; ethyl acetate / 20 °C / Inert atmosphere View Scheme
参考文献
Ren, Xuhong; Shen, Liu-Lan; Muraoka, Osamu; Cheng, Maosheng
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 3 p. 119 - 131
1064-06-8
[5,7-二乙酰氧基-2-(3,4-二乙酰氧基苯基)-4-氧代苯并吡喃-3-基]乙酸酯
→
反应条件
482-35-9
异槲皮苷
反应条件
1.1: potassium carbonate; potassium iodide / acetone / 120 h / Heating 2.1: sodium hydroxide / water; acetone / 3 h / 0 °C / Inert atmosphere 2.2: 0.5 h / 0 °C / Inert atmosphere 3.1: potassium carbonate / N,N-dimethyl-formamide / 32 h / 20 °C / Inert atmosphere 4.1: sodium methylate / methanol / 9.5 h / 20 °C / Inert atmosphere 5.1: palladium 10 on activated carbon; hydrogen / ethanol; ethyl acetate / 20 °C / Inert atmosphere View Scheme
参考文献
Ren, Xuhong; Shen, Liu-Lan; Muraoka, Osamu; Cheng, Maosheng
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 3 p. 119 - 131
78386-01-3
→
反应条件
482-35-9
异槲皮苷
反应条件
1.1: sodium hydroxide / water; acetone / 3 h / 0 °C / Inert atmosphere 1.2: 0.5 h / 0 °C / Inert atmosphere 2.1: potassium carbonate / N,N-dimethyl-formamide / 32 h / 20 °C / Inert atmosphere 3.1: sodium methylate / methanol / 9.5 h / 20 °C / Inert atmosphere 4.1: palladium 10 on activated carbon; hydrogen / ethanol; ethyl acetate / 20 °C / Inert atmosphere View Scheme
参考文献
Ren, Xuhong; Shen, Liu-Lan; Muraoka, Osamu; Cheng, Maosheng
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 3 p. 119 - 131
131021-81-3
→
反应条件
482-35-9
异槲皮苷
反应条件
1: sodium methylate / methanol / 9.5 h / 20 °C / Inert atmosphere 2: palladium 10 on activated carbon; hydrogen / ethanol; ethyl acetate / 20 °C / Inert atmosphere View Scheme
参考文献
Ren, Xuhong; Shen, Liu-Lan; Muraoka, Osamu; Cheng, Maosheng
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 3 p. 119 - 131
116973-12-7
→
反应条件
482-35-9
异槲皮苷
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 20 °C 2: sodium methylate / methanol; tetrahydrofuran / 6 h / 20 °C 3: palladium 10 on activated carbon; hydrogen / tetrahydrofuran; ethanol / 2 h / 20 °C / 750.08 Torr View Scheme
参考文献
Yamauchi, Kosei; Mitsunaga, Tohru; Batubara, Irmanida
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 3 p. 937 - 944
1332833-26-7
→
反应条件
482-35-9
异槲皮苷
反应条件
1: sodium methylate / methanol; tetrahydrofuran / 6 h / 20 °C 2: palladium 10 on activated carbon; hydrogen / tetrahydrofuran; ethanol / 2 h / 20 °C / 750.08 Torr View Scheme
参考文献
Yamauchi, Kosei; Mitsunaga, Tohru; Batubara, Irmanida
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 3 p. 937 - 944
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