1-苯基-7-噁双环[4.1.0]庚烷合成路线 （共 11 条）
反应条件
sulfuric acid in 1,4-dioxane; water T=25°C; 0.0333333 h; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 109, # 5 p. 1463 - 1469
反应条件
potassium hydroxide in 1,4-dioxane
参考文献
Berti,G. et al.
Tetrahedron, 1965 , vol. 21, p. 3277 - 3283
反应条件
oxygen P=4 Torr; Irradiationeffect of gas phase acid-induced ring opening; Product distributionMechanism;
参考文献
Crotti, P.; Macchia, F.; Pizzabiocca, A.; Renzi, G.; Speranza, M.
Tetrahedron Letters, 1987 , vol. 28, # 29 p. 3393 - 3396
反应条件
methane; hydrogen cation P=100 Torr; var. reagents and pressures,; Product distributionMechanism;
参考文献
Cecchi, P.; Pizzabiocca, A.; Renzi,G.; Chini, M.; Crotti, P.; et al.
Tetrahedron, 1989 , vol. 45, # 13 p. 4227 - 4234
反应条件
oxygen P=4 Torr; Irradiationeffect of gas phase acid-induced ring opening; Product distributionMechanism;
参考文献
Crotti, P.; Macchia, F.; Pizzabiocca, A.; Renzi, G.; Speranza, M.
Tetrahedron Letters, 1987 , vol. 28, # 29 p. 3393 - 3396
反应条件
lithium borohydride; borane-THF in tetrahydrofuran Ambient temperatureselective LiBH4*BH3 reduction of epoxides; cis-trans ratio; retention of configuration; Product distribution;
参考文献
Lynch; Choi; Churchill; Volante; Reamer; Ball
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 9223 - 9228
反应条件
1: bis(cyclopentadienyl)dimethyltitanium / tetrahydrofuran / 16 h / Inert atmosphere; Reflux 2: water; potassium carbonate / tetrahydrofuran; acetone / 16 h / Inert atmosphere View Scheme
参考文献
Gansaeuer, Andreas; Klatte, Max; Braendle, Gerhard M.; Friedrich, Joachim
Angewandte Chemie - International Edition, 2012 , vol. 51, # 35 p. 8891 - 8894
反应条件
formic acid; triethylamine; Pd0-EnCatTM in ethyl acetate
T=23°C; 7 h;
参考文献
Ley, Steven V.; Mitchell, Claire; Pears, David; Ramarao, Chandrashekar; Yu, Jin-Quan; Zhou, Wuzong
Organic Letters, 2003 , vol. 5, # 24 p. 4665 - 4668
反应条件
lithium borohydride; borane-THF in tetrahydrofuran
Ambient temperatureselective LiBH4*BH3 reduction of epoxides; cis-trans ratio; retention of configuration; Product distribution;
参考文献
Lynch; Choi; Churchill; Volante; Reamer; Ball
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 9223 - 9228
反应条件
aluminium trichloride in diethyl ether
参考文献
Guyon,R.; Villa,P.
Bulletin de la Societe Chimique de France, 1975 , p. 2593 - 2598
