2-羟基-3-甲基-1,4-萘醌合成路线 (共 82 条)
反应条件
formic acid in ethanol; water
T=200°C; P=155.149 - 155149 Torr; 3 h; chemoselective reaction;
参考文献
Ferreira, Sabrina Baptista; Rodriguesdarocha, David; Carneiro, Jose Walkimar M.; Santos, Wilson Costa; Ferreira, Vitor Francisco
Synlett, 2011 , # 11 p. 1551 - 1554
反应条件
sulfuric acid; silica gel
T=70°C; 0.133333 h;
参考文献
Zhu, Rui; Xing, Lixin; Wang, Xinyan; Cheng, Chuanjie; Liu, Bo; Hu, Yuefei
Synlett, 2007 , # 14 p. 2267 - 2271
反应条件
copper(II) sulfate
T=50°C; 2.5 h;
参考文献
Bansal; Thapliyal; Khanna
Synthetic Communications, 1995 , vol. 25, # 11 p. 1669 - 1675
反应条件
aluminum oxide; potassium fluoride; oxygen in methanol
T=25°C; oxidative saponification;
参考文献
Villemin; Bar; Hammadi; Hachemi
Journal of Chemical Research - Part S, 2000 , # 7 p. 356 - 358
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=20°C; Methylation; cross coupling; Stille coupling; 12 h;
参考文献
Stagliano, Kenneth W.; Malinakova, Helena C.
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 8034 - 8040
参考文献
Fieser; Oxford
Journal of the American Chemical Society, 1942 , vol. 64, p. 2063
参考文献
Syntex (U.S.A.) Inc.
Patent: US5091558 A1, 1992 ;
反应条件
sodium hydroxide; air; water
参考文献
Kuroda
Proceedings of the Imperial Academy (Tokyo), 1939 , vol. 15, p. 226,227
Journal of the Scientific Research Institute, Tokyo, 1951 , vol. 45, p. 166,167
反应条件
Fremy’s salt in methanol; water
0.5 h;
参考文献
Coll, Gloria; Morey, Jeroni; Costa, Antoni; Saa,Jose M.
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5345 - 5348
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
16 h; Ambient temperature;
参考文献
Stagliano, Kenneth W.; Malinakova, Helena C.
Tetrahedron Letters, 1997 , vol. 38, # 38 p. 6617 - 6620