2-乙基吡啶 1-氧化物合成路线 （共 13 条）
反应条件
1.1: 75.3 percent / HNO3; H2SO4 / 100 °C
2.1: 85 percent / HCl / H2O / 160 °C
3.1: Ac2O / 4 h / 110 °C
3.2: 54 percent / HCl / H2O / 2 h / 80 °C
4.1: 58 percent / H2SO4 / 90 °C
View Scheme
参考文献
Zhang, Christiana Xin; Liang, Hong-Chang; Kim, Eun-il; Shearer, Jason; Helton, Matthew E.; Kim, Eunsuk; Kaderli, Susan; Incarvito, Christopher D.; Zuberbuehler, Andreas D.; Rheingold, Arnold L.; Karlin, Kenneth D.
Journal of the American Chemical Society, 2003 , vol. 125, # 3 p. 634 - 635
反应条件
1: sulfuric acid; nitric acid
2: iron; concentrated aqueous HCl; acetic acid
View Scheme
参考文献
Kutscherowa et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 915,918; engl. Ausg. S. 898
反应条件
N,N-dimethylcarbamoyl chloride in 1-nitroethane
T=20°C; 72 h;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1424336 A1, 2004 ;
Location in patent: Page 108 ;
