N-3-丁烯-1-基-4-甲基-N-2-丙烯-1-基苯磺酰胺合成路线 （共 4 条）
反应条件
potassium carbonate in acetonitrile
6 h; Heating;
参考文献
Terada, Yukiyoshi; Arisawa, Mitsuhiro; Nishida, Atsushi
Angewandte Chemie - International Edition, 2004 , vol. 43, # 31 p. 4063 - 4067
反应条件
1: 100 percent / K2CO3 / acetonitrile / 1.5 h / Heating
2: 306.2 mg / TFA / CH2Cl2 / 40 h / 20 °C
3: 89 percent / K2CO3 / acetonitrile / 6 h / Heating
View Scheme
参考文献
Terada, Yukiyoshi; Arisawa, Mitsuhiro; Nishida, Atsushi
Angewandte Chemie - International Edition, 2004 , vol. 43, # 31 p. 4063 - 4067
反应条件
1: 306.2 mg / TFA / CH2Cl2 / 40 h / 20 °C
2: 89 percent / K2CO3 / acetonitrile / 6 h / Heating
View Scheme
参考文献
Terada, Yukiyoshi; Arisawa, Mitsuhiro; Nishida, Atsushi
Angewandte Chemie - International Edition, 2004 , vol. 43, # 31 p. 4063 - 4067
反应条件
1: With 1-n-butyl-3-methylimidazolium hexafluorophosphate in dichloromethane
T=40°C; 1 h; Inert atmosphere;
2: With hydrogen in isopropyl alcohol
T=20°C; P=760.051 Torr; 0.5 h; Inert atmosphere;
参考文献
Lee, Sujin; Shin, Ju Yeon; Lee, Sang-Gi
Chemistry - An Asian Journal, 2013 , vol. 8, # 9 p. 1990 - 1993
