2,4,5－三苯基咪唑合成路线 （共 149 条）
参考文献
Franklin
Journal of the American Chemical Society, 1934 , vol. 56, p. 568,571
反应条件
in benzonitrile byproducts: 2,3,5,6-tetraphenylpyrazine; conventional Schlenk technique; PhCN added with stirring to Tm compd.; 5min; concd.; crystd. for 24 h; THF added to mother liquor; 1 h; decante d; solvent removed from soln.; MeOH added; pptd. (20°C, 24 h); MeOH removed from soln.; pptd. by H2O; crystals after crystn. sepd. by decantation, washed with PhCN, dried (TmI3(PhCN)4); ppt. of Tm-THF complex washed with cold THF, dried in vac.; ppt. after H2O addition sepd. by centrifuging, washed with ether, dried (TmI(OH)2(H2O)5); elem. anal.;
参考文献
Balashova; Khoroshenkov; Kusyaev; Eremenko; Aleksandrov; Fukin; Bochkarev
Russian Chemical Bulletin, 2004 , vol. 53, # 4 p. 825 - 829
反应条件
neodymium(II) diiodide in tetrahydrofuran Product distribution; Further Variations:Reagents;
参考文献
Balashova; Khoroshenkov; Kusyaev; Eremenko; Aleksandrov; Fukin; Bochkarev
Russian Chemical Bulletin, 2004 , vol. 53, # 4 p. 825 - 829
反应条件
Yield given. Further byproducts given;
参考文献
Compagnon, Paul-Luis; Gasquez, Francoise; Compagnon, Odette; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1982 , vol. 91, # 11 p. 931 - 946
反应条件
Further byproducts given;
参考文献
Compagnon, Paul-Luis; Gasquez, Francoise; Compagnon, Odette; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1982 , vol. 91, # 11 p. 931 - 946
反应条件
in benzene 1.5 h; Irradiationirradiation in methanol; other imidazolyl-1,2-dibenzoylethylenes; MechanismProduct distribution;
参考文献
Barik, Rabindra; Bhattacharyya, Kankan; Das, Paritosh K.; George, Manapurathu V.
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3420 - 3428
参考文献
Wenkert; Mekler
Journal of the American Chemical Society, 1956 , vol. 78, p. 2213,2216
反应条件
T=100°C; dl-benzoin;
参考文献
Erdmann
Justus Liebigs Annalen der Chemie, 1865 , vol. 135, p. 182
Full Text Show Details
Laurent
Journal fuer Praktische Chemie (Leipzig), 1845 , vol. <1> 36, p. 5
Berzelius' Jahresber., vol. 26, p. 667
Full Text Show Details
Japp; Wilson
Journal of the Chemical Society, 1886 , vol. 49, p. 825,831
反应条件
T=275°C; 1 h; Mechanism;
参考文献
Marshalkin, M. F.; Yakhontov, L. N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 2273 - 2276
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 12 p. 2577 - 2580
反应条件
T=240 - 250°C; 0.5 h; other 1-aroylamino-4,5-diaryl-1,2,3-triazoles, also in the presence of p-CH3C6H4CN; MechanismProduct distribution;
参考文献
Hadjiantoniou-Maroulis; Charalambopoulos; Maroulis
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 4 p. 891 - 894
