2,4,5－三苯基咪唑合成路线 （共 149 条）
反应条件
1: 96 percent / Heating 2: 10percent H2SO4 / ethanol / 20 h / Heating View Scheme
参考文献
Giammanco, Lorenzo; Invidiata, Francesco Paolo
Heterocycles, 1985 , vol. 23, # 6 p. 1459 - 1464
反应条件
T=280°C; P=0.045 Torr; 0.25 h; Gas phase;
参考文献
Ibrahim, Maher R.; Al-Azemi, Talal F.; Al-Etabi, Alya; El-Dusouqui, Osman M.E.; Al-Awadi, Nouria A.
Tetrahedron, 2010 , vol. 66, # 23 p. 4243 - 4250
反应条件
benzil T=149.85°C; 0.5 h;
参考文献
Vazquez Garcia, Rosa A.; Bernes, Sylvain; Gutierrez Perez, Rene; Martinez Garcia, Marcos
Acta Crystallographica Section C: Crystal Structure Communications, 2002 , vol. 58, # 10 p. o619-o620
反应条件
1: bis(η3-allyl-μ-chloropalladium(II)); tri-tert-butyl phosphine / acetonitrile / 55 °C / 3040.2 Torr / Inert atmosphere; sealed glass reaction tube 2: Pearlman's catalist; hydrogen; acetic acid / 60 °C / 2280.15 Torr / Inert atmosphere; Teflon-sealed glass reaction vessel 3: sulfur / dimethyl sulfoxide / 18 h / 75 °C / Inert atmosphere View Scheme
参考文献
Bontemps, Sebastien; Quesnel, Jeffrey S.; Worrall, Kraig; Arndtsen, Bruce A.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 38 p. 8948 - 8951
反应条件
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / methanol; toluene; water / 3 h / 120 °C / |Inert atmosphere 2: potassium tert-butylate; oxygen / tetrahydrofuran; dimethyl sulfoxide / 16 h / 20 °C View Scheme
参考文献
Recnik, Lisa-Maria; Abd El Hameid, Mohammed; Haider, Maximilian; Schnuerch, Michael; Mihovilovic, Marko D.
Synthesis (Germany), 2013 , vol. 45, # 10 art. no. SS-2012-Z0934-OP, p. 1387 - 1405
反应条件
in tetrahydrofuran 1) -65 deg C, 2 h, 2) r.t., 12 h;
参考文献
Kauffmann, Thomas; Busch, Alfred; Habersaat, Kai; Koeppelmann, Edgar
Chemische Berichte, 1983 , vol. 116, # 2 p. 492 - 499
参考文献
Spassow et al.
Godisnik Univ. SofiaChem.Abstr., 49 Chimija <1954/55> 119, 123 1957 , p. 12075
反应条件
potassium ethanolate T=200°C; 0.5 h; Mechanism;
参考文献
Marshalkin, M. F.; Yakhontov, L. N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 2273 - 2276
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 12 p. 2577 - 2580
参考文献
Koetz; Wunstorf
Journal fuer Praktische Chemie (Leipzig), 1913 , vol. <2> 88, p. 528
参考文献
Koetz; Wunstorf
Journal fuer Praktische Chemie (Leipzig), 1913 , vol. <2> 88, p. 528
