2,4,5－三苯基咪唑合成路线 （共 149 条）
反应条件
in tetrahydrofuran conventional Schlenk technique; PhCN added with stirring to NdI2; 5 min;PhCN removed in vac.; THF added; pptd. for 1 h; decanted; solvent remov ed from mother liquor; MeOH added; pptd. (20°C, 20 h); MeOH removed from soln.; pptd. by adding H2O; ppt. after decantation washed with cold THF, dried in vac. (NdI3(thf)3);ppt. after H2O addition sepd. by centrifuging, dried (NdI(OH)2(H2O)5); elem. anal.;
参考文献
Balashova; Khoroshenkov; Kusyaev; Eremenko; Aleksandrov; Fukin; Bochkarev
Russian Chemical Bulletin, 2004 , vol. 53, # 4 p. 825 - 829
反应条件
in various solvent(s) 24 h; Heating;
参考文献
Collibee, William L.; Anselme, Jean-Pierre
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 8 p. 655 - 662
参考文献
Howard et al.
Journal of the American Chemical Society, 1932 , vol. 54, p. 3628,3635
参考文献
Howard et al.
Journal of the American Chemical Society, 1932 , vol. 54, p. 3628,3635
反应条件
lithium azide in acetonitrile 20 h; Ambient temperature;
参考文献
Jarvis, Bruce B.; Stahly, G.Patrick
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2604 - 2609
反应条件
in isopropyl alcohol 57 h; Ambient temperatureIrradiation;
参考文献
Nagy, Jozsef; Rapp, Rudolf; Alexovics, Maria; Doepp, Dietrich; Nyitrai, Jozsef; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 6 p. 661 - 666
参考文献
Strain
Journal of the American Chemical Society, 1927 , vol. 49, p. 1568
反应条件
in diethyl ether 8 h; Heating; Product distribution;
参考文献
Tanaseichuk, B. S.; Belozerov, A. I.; Sanaeva, E. P.; Butin, K. P.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 494 - 497
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 561 - 565
反应条件
bei der Destillation;
参考文献
Brunner
Justus Liebigs Annalen der Chemie, 1869 , vol. 151, p. 133
反应条件
in diethyl ether 8 h; Heating; Product distribution;
参考文献
Tanaseichuk, B. S.; Belozerov, A. I.; Sanaeva, E. P.; Butin, K. P.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 494 - 497
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 561 - 565
