2,3,4,5,6-五甲基苯甲醇合成路线 （共 30 条）
反应条件
hydrogenchloride; epoxysulfonyl fluoride; lead dioxide 1. -75 grad C 2. - 40 grad C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rudenko, A. P.; Zarubin, M. Ya.; Fedorova, E. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1762 - 1772
反应条件
3,3-dimethyldioxirane in acetone 24 h; Ambient temperatureother reaction time, temperature, effect of amount of oxidant. effect of additives; Product distribution;
参考文献
Murray, Robert W.; Singh, Megh; Rath, Nigam
Journal of Organic Chemistry, 1997 , vol. 62, # 25 p. 8794 - 8799
反应条件
hydrogenchloride; epoxysulfonyl fluoride; lead dioxide 1. 75 grad C, 2- 3,5 h 2. - 60 grad C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rudenko, A. P.; Zarubin, M. Ya.; Fedorova, E. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1762 - 1772
反应条件
1-chloro-piperidine Ambient temperature;
参考文献
Smith, John R. Lindsay; McKeer, Linda C.; Taylor, Jonathan M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1537 - 1544
反应条件
in acetonitrile Irradiationvarious reaction conditions, kinetic isotope effect; Product distributionMechanism;
参考文献
Masnovi, J. M.; Sankararaman, S.; Kochi, J. K.
Journal of the American Chemical Society, 1989 , vol. 111, # 6 p. 2263 - 2276
反应条件
epoxysulfonyl fluoride; lead dioxide T=-75 - -70°C; 2 h; different conc. PbO2, different time, decomposition reagent CH3OH or HCl conc.; MechanismProduct distribution;
参考文献
Rudenko, A. P.; Zarubin, M. Ya.; Fedorova, E. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1762 - 1772
反应条件
in various solvent(s) T=20°C; 24 h; Irradiationother time; Product distribution;
参考文献
Eberson, Lennart; Hartshorn, Michael P.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 12 p. 1121 - 1136
反应条件
ammonium nitrate; hydrogenchloride; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen in water; acetonitrile T=60°C; 7 h; Green chemistry;
参考文献
Prebil, Rok; Stavber, Gaj; Stavber, Stojan
European Journal of Organic Chemistry, 2014 , vol. 2014, # 2 p. 395 - 402
反应条件
indium(III) chloride tetrahydrate in 1,2-dichloro-ethane T=80°C; 8 h; Sealed tube;
参考文献
Chen, Song-Jie; Hua, Ruimao
Letters in Organic Chemistry, 2010 , vol. 7, # 1 p. 61 - 63
反应条件
3,3-dimethyldioxirane in acetone
72 h; Ambient temperature;
参考文献
Murray, Robert W.; Singh, Megh; Rath, Nigam
Journal of Organic Chemistry, 1997 , vol. 62, # 25 p. 8794 - 8799
